Citation: Xin-Juan Wang, Yao-Hang Cheng, Xin-Yan Lv, Li-Ye Liang, Guang-Hui An, Guang-Ming Li. Ruthenium-catalyzed alkylarylation of alkenes via para-selective C-H functionalization of unprotected anilines[J]. Chinese Chemical Letters, ;2026, 37(8): 112154. doi: 10.1016/j.cclet.2025.112154 shu

Ruthenium-catalyzed alkylarylation of alkenes via para-selective C-H functionalization of unprotected anilines

Xin-Juan Wang ^a ,
Yao-Hang Cheng ^a ,
Xin-Yan Lv ^a ,
Li-Ye Liang ^a ,
Guang-Hui An ^{a, b, *,} ,
Guang-Ming Li ^{a, *,}

a.
Key Laboratory of Functional Inorganic Material Chemistry (MOE), School of Chemistry and Materials Science, Heilongjiang University, Harbin 150080, China
b.
College of Materials Science and Chemical Engineering, Harbin Engineering University, Harbin 150001, China

chemagh@163.com

gmli@hlju.edu.cn

Received Date: 6 April 2025
Revised Date: 6 November 2025
Accepted Date: 21 November 2025
Available Online: 22 November 2025

Figures(6)

Metal-catalyzed alkylarylation of two carbon−carbon (C-C) bonds across vicinal C(sp²) sites in olefins can provide access to diverse combinatorial chemical space. Pre-activated arenes are often used as aryl sources, but the direct utilization of Csp²−H bond instead of pre-activated arenes remains underdeveloped. Herein, ruthenium-catalyzed alkylarylation of alkenes via para-selective C-H functionalization of unprotected aniline has been reported. It bears good functional group tolerance and enables late functionalization of complex natural products. Evaluation of cone angle and minimum percent buried volume help to determine the optimal ligand. The mechanism studies reveal the dissociation of p-cymene during the catalytic cycle which triggers the redox processes for radical generation.
- Alkylarylation,
- Three component reaction,
- para-Selectivity,
- Ru-catalyzed
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