Citation: Kun Zhao, Bing Chen, Luwen Liang, Yaze Chen, Shan Yao, Qun Peng, Yuhao Liu, Bin Han. Microenvironment engineering of covalent organic frameworks for hydrogen peroxide synthesis via photocatalytic oxygen reduction[J]. Chinese Chemical Letters, ;2026, 37(6): 112032. doi: 10.1016/j.cclet.2025.112032 shu

Microenvironment engineering of covalent organic frameworks for hydrogen peroxide synthesis via photocatalytic oxygen reduction

Kun Zhao ^a ,
Bing Chen ^a ,
Luwen Liang ^a ,
Yaze Chen ^b ,
Shan Yao ^{a, *,} ,
Qun Peng ^a ,
Yuhao Liu ^{b, *,} ,
Bin Han ^{a, *,}

a.
Guangdong Basic Research Center of Excellence for Ecological Security and Green Development, Key Laboratory for City Cluster Environmental Safety and Green Development of the Ministry of Education, School of Ecology, Environment and Resources, Guangdong University of Technology, Guangzhou 510006, China
b.
Pingyuan Laboratory, College of Chemistry, Zhengzhou University, Zhengzhou 450000, China

yaoshan97@gdut.edu.cn

yuhaoliu@zzu.edu.cn

hanbin@gdut.edu.cn

Received Date: 30 May 2025
Revised Date: 13 October 2025
Accepted Date: 27 October 2025
Available Online: 28 October 2025

Figures(7)

Hydrogen peroxide (H₂O₂) is a vital oxidant and a promising liquid fuel, serving as one of the 100 most essential chemicals. Covalent organic frameworks (COFs) have emerged as ideal candidates for pure H₂O₂ photosynthesis due to their fully designable structures and well-defined active sites. The microenvironment engineering of COFs presents exciting opportunities to optimize both selectivity and efficiency in H₂O₂ photosynthesis, while their precisely identifiable active sites enable rational design of next-generation high-performance COFs. Although significant progress has been made in regulating COFs’ active sites for H₂O₂ photosynthesis, a comprehensive review systematically analyzing this specific and significant area remains absent. Here, we provide a thorough overview of the recent advances and persistent challenges in the microenvironment engineering of COFs for H₂O₂ photosynthesis. To begin with, the basic principles of O₂-to-H₂O₂ photocatalytic conversion and outline general strategies for microenvironment engineering of COFs are presented. Subsequently, we critically examine the current research progress in this field. The urgent challenges and the future development of the microenvironment engineering of COFs in H₂O₂ photosynthesis are finally proposed. This review will provide valuable theoretical guidance for developing the next generation of COF photocatalysts that promote H₂O₂ photosynthesis.
- Covalent organic frameworks,
- Microenvironment engineering,
- Photocatalysis,
- Oxygen reduction,
- Hydrogen peroxide
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沈阳化工大学材料科学与工程学院沈阳 110142