Citation: Yufeng Gan, Deqian Zeng, Shunyan Ning, Ningchao Zheng, Xinpeng Wang, Yuezhou Wei, Jizhou Jiang. Synergistic H₂ production and tetracycline degradation: Unveiling the mechanism of a one-pot synthesized CeO₂/CdS photocatalyst[J]. Chinese Chemical Letters, ;2026, 37(5): 111717. doi: 10.1016/j.cclet.2025.111717 shu

Synergistic H₂ production and tetracycline degradation: Unveiling the mechanism of a one-pot synthesized CeO₂/CdS photocatalyst

Yufeng Gan ^{a, b} ,
Deqian Zeng ^{a, *,} ,
Shunyan Ning ^a ,
Ningchao Zheng ^a ,
Xinpeng Wang ^b ,
Yuezhou Wei ^a ,
Jizhou Jiang ^{c, *,}

a.
School of Nuclear Science and Technology, University of South China, Hengyang 421001, China
b.
School of Resources, Environment and Materials, Guangxi University, Nanning 530004, China
c.
School of Materials Science and Engineering, State Key Laboratory of Green and Efficient Development of Phosphorus Resources, Engineering Research Center of Phosphorus Resources Development and Utilization of Ministry of Education, Key Laboratory of Green Chemical Engineering Process of Ministry of Education, Hubei Key Laboratory of Plasma Chemistry and Advanced Materials, Novel Catalytic Materials of Hubei Engineering Research Center, Wuhan Institute of Technology, Wuhan 430205, China

dqzeng@usc.edu.cn

027wit@163.com

Received Date: 5 April 2025
Revised Date: 12 August 2025
Accepted Date: 12 August 2025
Available Online: 14 August 2025

Figures(11)

Coupling photocatalytic H₂ generation with antibiotic degradation offers a promising strategy for addressing energy and environmental challenges, leveraging the synergistic benefits of these processes. Herein, a novel heterojunction photocatalyst consisting of ultrafine CeO₂ nanoparticles anchored onto CdS nanosheets was prepared using a simple one-pot in-situ hydrothermal method, enabling the simultaneous photocatalytic H₂ generation and tetracycline (TC) degradation. The H₂ generation efficiency of the optimal CeO₂/CdS (CC-0.10) is 3544 µmol g^-1 h^-1, which surpasses pure CdS by 29.3 times. Additionally, TC is degraded by CC-0.10 at a rate constant (k value) of 0.0352 min^-1, 2.73 times faster than CdS (0.0129 min^-1). The free radical quenching and electron spin resonance experiments revealed the active involvement of ^•OH and ^•O₂^- radicals in the TC degradation process. Moreover, the unique CeO₂/CdS heterojunction photocatalyst was also effective in degrading TC wastewater with an H₂ yield of 1374 µmol g^-1 h^-1, displaying its dual performance in simultaneously degrading antibiotic wastewater and producing H₂. The CeO₂/CdS type Ⅱ charge transfer mechanism is confirmed by XPS, EPR, KPFM, fs-TAS, and DFT calculations. This work introduces a promising approach to constructing rare-earth oxide/metal sulfide nanocomposites for addressing the interconnected challenges of energy production and environmental pollution.
- In-situ hydrothermal method,
- Synergistic,
- Photocatalytic H₂ production,
- TC degradation,
- Charge transfer
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Synergistic H2 production and tetracycline degradation: Unveiling the mechanism of a one-pot synthesized CeO2/CdS photocatalyst

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Synergistic H₂ production and tetracycline degradation: Unveiling the mechanism of a one-pot synthesized CeO₂/CdS photocatalyst