Citation: Huiyuan Deng, Na Zhao, Junjie You, Zhicheng Pan, Bo Xing, Yuling Ye, Bo Lai, Yuxi Wang, Tongrui Lu, Xiaonan Liu. Removal of bisphenol a through peroxymonosulfate activation with N-doped graphite carbon spheres coated cobalt nanoparticles catalyst: Synergy of nonradicals[J]. Chinese Chemical Letters, ;2025, 36(8): 110650. doi: 10.1016/j.cclet.2024.110650 shu

Removal of bisphenol a through peroxymonosulfate activation with N-doped graphite carbon spheres coated cobalt nanoparticles catalyst: Synergy of nonradicals

Huiyuan Deng ^{a, b, c} ,
Na Zhao ^a ,
Junjie You ^{a, b, c, *,} ,
Zhicheng Pan ^{b, e} ,
Bo Xing ^{a, b, c} ,
Yuling Ye ^{a, b, c} ,
Bo Lai ^d ,
Yuxi Wang ^a ,
Tongrui Lu ^a ,
Xiaonan Liu ^{a, b, c, *,}

a.
School of Chemical Engineering, Sichuan University of Science and Engineering, Zigong 643000, China
b.
National Engineering Laboratory of Circular Economy, Sichuan University of Science and Engineering, Zigong 643000, China
c.
Sichuan Engineering Technology Research Center for High Salt wastewater Treatment and Resource Utilization, Sichuan University of Science and Engineering, Zigong 643000, China
d.
Sino-German Centre for Water and Health Research, Sichuan University, Chengdu 610065, China
e.
Water Safety and Water Pollution Control Engineering Technology Research Center in Sichuan Province, Haitian Water Group Co., Ltd., Chengdu 610041, China

18782938242@163.com

lxn@suse.edu.com

Received Date: 2 August 2024
Revised Date: 9 October 2024
Accepted Date: 13 November 2024
Available Online: 14 November 2024

Figures(6)

N-doped graphite carbon sphere coated cobalt nanoparticle catalyst (Co@C-N-900), prepared by solvothermal-calcination method, is applied to activate peroxymonosulfate (PMS) for bisphenol A (BPA) elimination. The outcomes demonstrate that the Co@C-N-900 could effectively activate PMS, thereby causing efficient removal of BPA in water. In addition, the Co@C-N-900/PMS system also has the advantages of low metal leaching, applicability in high salinity environments, good selectivity and stability. Further investigations using electron paramagnetic resonance, chronoamperometry, and quenching experiments demonstrated that the Co@C-N-900/PMS system is a typical non-radical route with singlet oxygen (¹O₂) as the main reactive oxygen species (ROS). Density functional theory calculations (DFT) indicate that N-doping can effectively regulate the charge distribution on the catalyst surface, generating acidic/alkaline sites favorable for PMS adsorption and activation. Furthermore, it also can enhance the interaction and charge transfer capacity between the Co@C-N-900 and PMS. Lastly, LC-QTOF-MS/MS analysis revealed two possible BPA degradation pathways: (1) ¹O₂ attacked the isopropyl group in BPA between the two phenyl groups, causing β-scission to occur. (2) Following the oxidation of the hydroxyl group in the aromatic ring of BPA, ¹O₂ could cause further β-scission. The prepared Co@C-N-900 catalyst is a very promising catalyst, which would offer a workable remedy for treating water pollution.
- Co-based catalyst,
- Nitrogen doped graphite,
- Peroxymonosulfate,
- Non-radical pathway,
- DFT calculations
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