Citation: Xin Wang, Jianping Meng, Dongyang Zhao, Shi Tang, Kai Sun. Synthesis and applications of thiosulfonates and selenosulfonates as free-radical reagents[J]. Chinese Chemical Letters, ;2023, 34(4): 107736. doi: 10.1016/j.cclet.2022.08.016 shu

Synthesis and applications of thiosulfonates and selenosulfonates as free-radical reagents

Xin Wang ^{a, *,} ,
Jianping Meng ^a ,
Dongyang Zhao ^a ,
Shi Tang ^b ,
Kai Sun ^{a, *,}

a.
College of Chemistry and Chemical Engineering, Yantai University, Yantai 264005, China
b.
College of Chemistry and Chemical Engineering, Jishou University, Jishou 416000, China

Author Bio: Xin Wang was born in Heilongjiang, China and received her MS degree from Northeast Normal University in 2012. In July 2013, she joined the College of Chemistry and Chemical Engineering, Anyang Normal University. In 2019, she pursued her Ph.D. degree in Zhengzhou University. Her research program is drug design, structural identification and structural modification of natural products
Jianping Meng was born in Heilongjiang Province, China in 1994. In 2014, she began her studies at the School of Science of Heihe University. In 2019, she pursued her MS degree under the supervision of Kai Sun in YanTai University. Her current research is focused on green synthetic chemistry

Kai Sun was born in Shanxi, China in 1983. He received his Ph.D. degree in organic chemistry from Northeast Normal University in 2013 under the supervision of Prof. Qian Zhang. In July 2020, he joined the College of Chemistry and Chemical Engineering, YanTai University, where he is an associate professor. His current research is focused on radical C–H functionalization and green synthetic chemistry

wangx933@nenu.edu.cn

sunk468@nenu.edu.cn

Received Date: 13 June 2022
Revised Date: 26 July 2022
Accepted Date: 5 August 2022
Available Online: 11 August 2022

Figures(32)

Chalcogenative sulfones (thiosulfonates and selenosulfonates), as reactants for organic transformations, are widely used and interesting because of their potential to react with nucleophiles, electrophiles, and free radicals. As stable radical reagents, the synthesis and applications of chalcogenative sulfones have opened up a novel pathway to synthesize many kinds of compounds containing sulfur or selenium motifs. However, despite the numerous recent works on the synthesis and applications of thiosulfonates and selenosulfonates as radical reagents, no review has yet provided a summary of the literature. In this paper, we aim to review the synthesis and applications strategies of chalcogenative sulfones as radical reagents reported over the past several decades. Different types of catalysis are discussed in this review: (ⅰ) metal catalysis; (ⅱ) visible-light catalysis; (ⅲ) synergistic catalysis; and (ⅲⅰ) other types. Concurrently, in visible-light catalysis and metallaphotoredox catalysis sections, we highlight that developing relatively environmentally friendly synthetic methods in this area is always a great challenge, but also a persistent pursuit. Finally, the scopes, limitations, mechanisms, and existing problems of some reactions are described briefly.
- Chalcogenative sulfones,
- Radical,
- Synthesis,
- Applications,
- Mechanisms
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沈阳化工大学材料科学与工程学院沈阳 110142