Citation: Xing-Li Liu, Chun Wang, Qiu-Hua Wu, Zhi Wang. Preconcentration of chlorophenols in water samples using threedimensional graphene-based magnetic nanocomposite as absorbent[J]. Chinese Chemical Letters, ;2014, 25(8): 1185-1189. doi: 10.1016/j.cclet.2014.03.030 shu

Preconcentration of chlorophenols in water samples using threedimensional graphene-based magnetic nanocomposite as absorbent

1.
College of Science, Agricultural University of Hebei, Baoding 071001, China

Corresponding author: Qiu-Hua Wu,
Received Date: 10 December 2013
Available Online: 28 February 2014
Fund Project: Financial supports from the National Natural Science Foundation of China (No. 31171698) (No. 31171698)the Natural Science Foundations of Hebei (No. B2012204028) are gratefully acknowledged. (No. ZD20131033)

In this paper, a novelmagnetic solid-phase extraction method using three-dimensional graphene-based magnetic nanocomposite as adsorbent for the preconcentration of several chlorophenols from water samples prior to high-performance liquid chromatography analysis was developed. Various experimental parameters were investigated. Under the optimum conditions, the enrichment factors of the method were in the range of 186-312, and the limit of detection (S/N=3) was 0.10 ng/mL. The recoveries of the method were in the range between 85.1% and 101.2%. The developed method has been successfully applied to the determination of chlorophenols in environmental water samples.
- Three-dimensional graphene,
- Magnetic adsorbent,
- High performance liquid chromatography,
- Chlorophenols,
- Water samples
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沈阳化工大学材料科学与工程学院沈阳 110142