Citation:
Wei Wang, Jie Zhang, LianHuan Han, DeZhi Yang, Dong Ping Zhan. Generation/collection mode of SECMwith combined probe[J]. Chinese Chemical Letters,
;2012, 23(1): 86-88.
doi:
10.1016/j.cclet.2011.09.015
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Here we report a novel generation/collection operation mode of scanning electrochemical microscopy, in which a theta micropipette was employed to support two adjacent water/1,2-dichloroethane interfaces separated by the thin central glass wall:one acts as the generator while the other as the collector. The generation current, collection current andcollection efficiencywere enhanced significantly when the tip approached to an insulate substrate.
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Keywords:
- SECM,
- Generation/collection mode,
- Combined probe
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