Citation: Yu Xia Da, Zhang Zhang, Zheng Jun Quan. Intermolecular cyclocondensation reaction of 3,4-dihydropyrimidine-2-thione under the Mitsunobu reaction conditions[J]. Chinese Chemical Letters, ;2011, 22(6): 679-682. doi: 10.1016/j.cclet.2010.12.041 shu

Intermolecular cyclocondensation reaction of 3,4-dihydropyrimidine-2-thione under the Mitsunobu reaction conditions

Key Laboratory of Eco-Environment-Related Polymer Materials, Ministry of Education, Gansu Key Laboratory of Polymer Materials, College of Chemistry and Chemical Engineering, Northwest Normal University, Lanzhou 730070, China

Received Date: 11 October 2010

Fund Project: We are thankful for the financial support from the National Nature Science Foundation of China (No.20902073)and Scientific and Technological Innovation Engineering program of Northwest Normal University (nwnu-kjcxgc-03-64)the Natural Science Foundation of Gansu Province (No.096RJZA116)

A self-intermolecular cyclocondensation reaction of 3,4-dihydropyrimidine-2-thione(DHPM)to give a novel tricyclic structure containing DHPM core in the presence of diethyl azodicarboxylate(DEAD)and triphenylphosphine(TPP)at room temperature is reported.
- Mitsunobu reaction,
- Cyclocondensation,
- 3,4-Dihydropyrimidine-2-thiones
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