引用本文:
Yan Wang, Qing Qiang Yao, Mu Zou Wang. High performance liquid chromatographic separation of clausenamide enantiomers with chiral-AGP stationary phase[J]. Chinese Chemical Letters,
2010, 21(7): 860-863.
doi:
10.1016/j.cclet.2010.01.024
Citation: Yan Wang, Qing Qiang Yao, Mu Zou Wang. High performance liquid chromatographic separation of clausenamide enantiomers with chiral-AGP stationary phase[J]. Chinese Chemical Letters, 2010, 21(7): 860-863. doi: 10.1016/j.cclet.2010.01.024
Citation: Yan Wang, Qing Qiang Yao, Mu Zou Wang. High performance liquid chromatographic separation of clausenamide enantiomers with chiral-AGP stationary phase[J]. Chinese Chemical Letters, 2010, 21(7): 860-863. doi: 10.1016/j.cclet.2010.01.024
High performance liquid chromatographic separation of clausenamide enantiomers with chiral-AGP stationary phase
摘要:
A method of high performance liquid chromatographic separation of clausenamide enantiomers with chiral-AGP (α1-acid glycoprotein)stationary phases has been established.The absolute configurations of (-)clausenamide and (+)clausenamide are 3S,4R,5R,6S and 3R,4S,5S,6R,respectively.The present method has been used to analyze the (-) clausenamide and (+) clausenamide and its analogues such as the major metabolite and synthetic derivatives of clansenamide.
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关键词:
- Enantiomers
- / (-)Clausenamide
- / (+)Clausenamide
- / Chiral-AGP
- / HPLC
English
High performance liquid chromatographic separation of clausenamide enantiomers with chiral-AGP stationary phase
Abstract:
A method of high performance liquid chromatographic separation of clausenamide enantiomers with chiral-AGP (α1-acid glycoprotein)stationary phases has been established.The absolute configurations of (-)clausenamide and (+)clausenamide are 3S,4R,5R,6S and 3R,4S,5S,6R,respectively.The present method has been used to analyze the (-) clausenamide and (+) clausenamide and its analogues such as the major metabolite and synthetic derivatives of clansenamide.
-
Key words:
- Enantiomers
- / (-)Clausenamide
- / (+)Clausenamide
- / Chiral-AGP
- / HPLC
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