引用本文:
Cheng Deng, Yong Cai Song, Ying De Wang, Yi He Li, Yong Peng Lei, Shu Wei Cao. A facile synthesis of 2,4,6-trichloroborazine from boron trichloride-dimethylsulfide complex and ammonium chloride[J]. Chinese Chemical Letters,
2010, 21(2): 135-138.
doi:
10.1016/j.cclet.2009.10.016
Citation: Cheng Deng, Yong Cai Song, Ying De Wang, Yi He Li, Yong Peng Lei, Shu Wei Cao. A facile synthesis of 2,4,6-trichloroborazine from boron trichloride-dimethylsulfide complex and ammonium chloride[J]. Chinese Chemical Letters, 2010, 21(2): 135-138. doi: 10.1016/j.cclet.2009.10.016
Citation: Cheng Deng, Yong Cai Song, Ying De Wang, Yi He Li, Yong Peng Lei, Shu Wei Cao. A facile synthesis of 2,4,6-trichloroborazine from boron trichloride-dimethylsulfide complex and ammonium chloride[J]. Chinese Chemical Letters, 2010, 21(2): 135-138. doi: 10.1016/j.cclet.2009.10.016
A facile synthesis of 2,4,6-trichloroborazine from boron trichloride-dimethylsulfide complex and ammonium chloride
摘要:
2,4,6-Trichloroborazine has been recognized as a desirable monomer for the preparation of high-performance boron nitride fibers through polymer derived ceramics route.So a high yield and facile synthesis of 2,4,6-trichloroborazine is essential in practice.Using boron trichloride-dimethylsulfide complex((CH3)2S·BCl3)and ammonium chloride(NH4Cl)as starting materials and toluene(C6H5CH3)as solvent,the synthesis of 2,4,6-trichloroborazine to give high yield is reported.(C)2009 Cheng Deng.Published by Elsevier B.V.on behalf of Chinese Chemical Society.All rights reserved.
English
A facile synthesis of 2,4,6-trichloroborazine from boron trichloride-dimethylsulfide complex and ammonium chloride
Abstract:
2,4,6-Trichloroborazine has been recognized as a desirable monomer for the preparation of high-performance boron nitride fibers through polymer derived ceramics route.So a high yield and facile synthesis of 2,4,6-trichloroborazine is essential in practice.Using boron trichloride-dimethylsulfide complex((CH3)2S·BCl3)and ammonium chloride(NH4Cl)as starting materials and toluene(C6H5CH3)as solvent,the synthesis of 2,4,6-trichloroborazine to give high yield is reported.(C)2009 Cheng Deng.Published by Elsevier B.V.on behalf of Chinese Chemical Society.All rights reserved.
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