Citation: Xue Jing Yang, Ya Ling Yang, Wei Zhen, Mou Sheng Liu, Jun Hong Chai. Synthesis and characterization of Al doped δ-laminar crystal sodium silicate[J]. Chinese Chemical Letters, ;2009, 20(4): 462-464. doi: 10.1016/j.cclet.2008.12.032 shu

Synthesis and characterization of Al doped δ-laminar crystal sodium silicate

a Faculty of Life Science and Technology, Kunming University of Science and Technology, Kunming 650224, China bKunming Fruit Business and Economics Co. Ltd., Kunming 650106, China

Received Date: 1 July 2008

An modified laminar crystal sodium silicate (Al-SKS-6) was synthesized by spray drying and high temperature crystallization using sodium silicate as silicon source, Al atom as inorganic source and hexadecyltrimethy ammonium bromide (CTMAB) as the structure template. The hydrothermal stability of product was at least 1 h. The synthesized material was characterized by XRD and SEM. The results indicated that shape and intensity of XRD diffraction peak at 2θ took changes, but raw material δ phase crystal form kept unchanged, and assured high Ca²⁺ and Mg²⁺ binding capacity of the products. The Ca²⁺ and Mg²⁺ binding capacity of product is up to 380 mg Ca/g and 410mg Mg/g respectively. It was found that the hole of product became smaller and appeared rod structure based on SEM. The hydrothermal stability was increased due to the pillaring of Al atom.
- Al doping,
- δ-Laminar crystal sodium silicate,
- Detergent builder,
- Stability
1. [1]
  Dong Xin Zhao , Zhong Xian Huang . Effect of arginine on stability of GST-ZNF191(243-368). Chinese Chemical Letters, 2007, 18(3): 355-356. doi: 10.1016/j.cclet.2007.01.017
2. [2]
  Xin Zhang , Hua-Yan Yang , Xiao-Jing Zhao , Yu Wang , Nan-Feng Zheng . The effects of surface ligands and counter cations on the stability of anionic thiolated M₁₂Ag₃₂ (M=Au, Ag) nanoclusters. Chinese Chemical Letters, 2014, 25(6): 839-843. doi: 10.1016/j.cclet.2014.05.027
3. [3]
  Quan Zhang , Zhou Ye , Shu-Ting Wang , Jian Yin . Facile one-pot synthesis of PEGylated monodisperse mesoporous silica nanoparticles with controllable particle sizes. Chinese Chemical Letters, 2014, 25(2): 257-260.
4. [4]
  Rong-Hui Lai , Ping-Jiang Dong , Yong-Li Wang , Jian-Bin Luo . Redispersible and stable amorphous calcium phosphate nanoparticles functionalized by an organic bisphosphate. Chinese Chemical Letters, 2014, 25(2): 295-298.
5. [5]
  Xue Mei Liao , Wei Chu , Yang Li , Fu Dong Zhou , Shi Zhong Luo . Effects of support pore size on new Cs_2.5H_0.5PW₁₂O₄₀/SiO₂ catalysts for the ring-opening polymerization of tetrahydrofuran. Chinese Chemical Letters, 2009, 20(3): 344-347. doi: 10.1016/j.cclet.2008.11.032
6. [6]
  Fang Yuan , Fu Chen , Qing Yu Xiang , Xuan Qin , Zhi Rong Zhang , Yuan Huang . Synthesis and characterization of HPMA copolymer-5-FU conjugates. Chinese Chemical Letters, 2008, 19(2): 137-140. doi: 10.1016/j.cclet.2007.10.035
7. [7]
  Juan Huang , Jian Wei Wang , Tao Gong , Zhi Rong Zhang . Synthesis and characterization of insulin-5-Fu conjugate,enabling insulin as multi-drug carder via dendritic approach. Chinese Chemical Letters, 2007, 18(3): 247-250. doi: 10.1016/j.cclet.2006.12.026
8. [8]
  Yong Fang Liang , Hai Yan Pan , Xiu Ling Zhu , Yao Xia Zhang , Xi Gao Jian . Studies on synthesis and property of novel acid-base proton exchange membranes. Chinese Chemical Letters, 2007, 18(5): 609-612. doi: 10.1016/j.cclet.2007.03.031
9. [9]
  Su Xiaodan , Tao Jun , Wang Qing , Xu Peng , Luo Wei , Dang Meng , Wu Jiang , Teng Zhaogang . Controlled PEGylation of periodic mesoporous organosilica nanospheres for improving their stability in physiological solutions. Chinese Chemical Letters, 2019, 30(4): 929-932. doi: 10.1016/j.cclet.2019.02.014
10. [10]
  Li Yuanyuan , Chen Haohua , Qu Lingbo , Bai Ruopeng , Lan Yu . Geometry, stability and aromaticity of β-diketiminate-coordinated alkaline-earth compounds. Chinese Chemical Letters, 2019, 30(12): 2249-2253. doi: 10.1016/j.cclet.2019.06.001
11. [11]
  Zhou Wentao , Chen Yihua , Zhou Huanping . Strategies to Improve the Stability of Perovskite-based Tandem Solar Cells. Acta Physico-Chimica Sinica, 2021, 37(4): 2009044-0. doi: 10.3866/PKU.WHXB202009044
12. [12]
  Qi Yan-Jie , Liu Jin-Hua , Zheng Wen-Xu , Li Xin-Xiong , Zheng Shou-Tian . A rare porous zinc phosphonocarboxylate framework with high thermal stability and interesting structural transformation. Chinese Chemical Letters, 2018, 29(6): 959-962. doi: 10.1016/j.cclet.2017.09.060
13. [13]
  Liu Meng , Li Zhihao , Li Yingxue , Chen Jiajia , Yuan Quan . Self-assembled nanozyme complexes with enhanced cascade activity and high stability for colorimetric detection of glucose. Chinese Chemical Letters, 2019, 30(5): 1009-1012. doi: 10.1016/j.cclet.2018.12.021
14. [14]
  Guo Weihua , Yao Xiaozhang , Peng Lingyi , Lin Bingqing , Kang Yongqiang , Gan Lin . Platinum monolayers stabilized on dealloyed AuCu core-shell nanoparticles for improved activity and stability on methanol oxidation reaction. Chinese Chemical Letters, 2020, 31(3): 836-840. doi: 10.1016/j.cclet.2019.06.018
15. [15]
  Sun Yue , Xiang Haiyan , Li Huimin , Yu Gang , Chen Hong , Liu Song . High stability three-dimensional porous PtSn nano-catalyst for ethanol electro-oxidation reaction. Chinese Chemical Letters, 2020, 31(9): 2491-2494. doi: 10.1016/j.cclet.2020.04.025
16. [16]
  Zheng Chao , Liu Aqiang , Bi Chenghao , Tian Jianjun . SCN-doped CsPbI₃ for Improving Stability and Photodetection Performance of Colloidal Quantum Dots. Acta Physico-Chimica Sinica, 2021, 37(4): 2007084-0. doi: 10.3866/PKU.WHXB202007084
17. [17]
  Li Yaohao , Clark Kimberly A. , Tan Zhongping . Methods for engineering therapeutic peptides. Chinese Chemical Letters, 2018, 29(7): 1074-1078. doi: 10.1016/j.cclet.2018.05.027
18. [18]
  Ahmad Sajjad , Guo Xin . Rapid development in two-dimensional layered perovskite materials and their application in solar cells. Chinese Chemical Letters, 2018, 29(5): 657-663. doi: 10.1016/j.cclet.2017.08.057
19. [19]
  . Synthesis and biological activities of (E)-β-farnesene analogues containing 1,2,3-thiadiazole. Chinese Chemical Letters, 2017, 28(2): 372-376. doi: 10.1016/j.cclet.2016.10.030
20. [20]
  Yang Yang , Duy Pham Ngoc , Yao Disheng , Zhu Huaiyong , Yarlagadda Prasad , Wang Hongxia . Inorganic p-type semiconductors and carbon materials based hole transport materials for perovskite solar cells. Chinese Chemical Letters, 2018, 29(8): 1242-1250. doi: 10.1016/j.cclet.2018.05.008

Get Citation

PDF

XML

Metrics

PDF Downloads(0)
Abstract views(124)
HTML views(2)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

Address：Zhongguancun North First Street 2,100190 Beijing, PR China Tel: +86-010-82449177-888

DownLoad: Full-Size Img PowerPoint

Return