One-pot synthesis of (Z)-4-(2-bromovinyl)benezenesulfonamides by microwave-induced simultaneous debrominative decarboxylation and sulfamation of anti-2,3-dibromo-3-(4-hlorosulfonylphenyl)propanoic acid

Wen Sheng Zhang Chun Xiang Kuang Qing Yang

引用本文: Wen Sheng Zhang,  Chun Xiang Kuang,  Qing Yang. One-pot synthesis of (Z)-4-(2-bromovinyl)benezenesulfonamides by microwave-induced simultaneous debrominative decarboxylation and sulfamation of anti-2,3-dibromo-3-(4-hlorosulfonylphenyl)propanoic acid[J]. Chinese Chemical Letters, 2009, 20(1): 48-51. doi: 10.1016/j.cclet.2008.10.004 shu
Citation:  Wen Sheng Zhang,  Chun Xiang Kuang,  Qing Yang. One-pot synthesis of (Z)-4-(2-bromovinyl)benezenesulfonamides by microwave-induced simultaneous debrominative decarboxylation and sulfamation of anti-2,3-dibromo-3-(4-hlorosulfonylphenyl)propanoic acid[J]. Chinese Chemical Letters, 2009, 20(1): 48-51. doi: 10.1016/j.cclet.2008.10.004 shu

One-pot synthesis of (Z)-4-(2-bromovinyl)benezenesulfonamides by microwave-induced simultaneous debrominative decarboxylation and sulfamation of anti-2,3-dibromo-3-(4-hlorosulfonylphenyl)propanoic acid

  • 基金项目:

    This work was supported by the Natural Science Foundation of Shanghai, China (No. 06ZR14085) and by the Scientific Research Foundation for the Returned Overseas Chinese Scholars, State Education Ministry.We would like to thank the Center for Instrumental Analysis, Tongji University, China.

摘要: One-pot simultaneous debrominative decarboxylation and sulfamation of anti-2,3-dibromo-3-(4-chlorosulfonylphenyl)propanoic acid in DMF (for alkyl amines) or DMF-pyridine (for aryl amines) using a diverse range of alkyl and aryl amines under microwave irradiation condition stereoselectively afforded (Z)-4-(2-bromovinyl)benzenesulfonamides in good yields.

English

  • 加载中
计量
  • PDF下载量:  2
  • 文章访问数:  811
  • HTML全文浏览量:  19
文章相关
  • 收稿日期:  2008-07-07
通讯作者: 陈斌, bchen63@163.com
  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

  1. 本站搜索
  2. 百度学术搜索
  3. 万方数据库搜索
  4. CNKI搜索

/

返回文章