Citation: Wen Sheng Zhang, Chun Xiang Kuang, Qing Yang. One-pot synthesis of (Z)-4-(2-bromovinyl)benezenesulfonamides by microwave-induced simultaneous debrominative decarboxylation and sulfamation of anti-2,3-dibromo-3-(4-hlorosulfonylphenyl)propanoic acid[J]. Chinese Chemical Letters, ;2009, 20(1): 48-51. doi: 10.1016/j.cclet.2008.10.004 shu

One-pot synthesis of (Z)-4-(2-bromovinyl)benezenesulfonamides by microwave-induced simultaneous debrominative decarboxylation and sulfamation of anti-2,3-dibromo-3-(4-hlorosulfonylphenyl)propanoic acid

a Department of Chemistry, Tongji University, Siping Road 1239, Shanghai 200092, China;
b Department of Chemistry, Jiaozuo Teachers'College, Jiaozuo 454001, China;
c School of Pharmacy, Fudan University, Yixueyuan Road 138, Shanghai 200032, China

Received Date: 7 July 2008

Fund Project: This work was supported by the Natural Science Foundation of Shanghai, China (No. 06ZR14085) and by the Scientific Research Foundation for the Returned Overseas Chinese Scholars, State Education Ministry.We would like to thank the Center for Instrumental Analysis, Tongji University, China.

One-pot simultaneous debrominative decarboxylation and sulfamation of anti-2,3-dibromo-3-(4-chlorosulfonylphenyl)propanoic acid in DMF (for alkyl amines) or DMF-pyridine (for aryl amines) using a diverse range of alkyl and aryl amines under microwave irradiation condition stereoselectively afforded (Z)-4-(2-bromovinyl)benzenesulfonamides in good yields.
- One-pot,
- Arylsulfonamide,
- (Z)-Arylvinyl bromide,
- Amine,
- Microwave irradiation
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