Citation: Fa Fu Yang, Li Ming Liu, Chao Hui Liu, Xiao Hua Zheng, Yu Guo. Synthesis of novel biscalixarene-tube containing two kinds of calix[4]arene derivative units[J]. Chinese Chemical Letters, ;2008, 19(1): 9-11. doi: 10.1016/j.cclet.2007.10.032 shu

Synthesis of novel biscalixarene-tube containing two kinds of calix[4]arene derivative units

College of Chemistry and Materials, Fujian Normal University, Fuzhou 350007, China

Received Date: 20 June 2007

Fund Project: Financial support from the National Natural Science Foundation of China(No.20402002), Fujian Natural Science Foundation of China(No.2006J0155) and Program for New Century Excellent Talents in University of Fujian Province were greatly acknowledged.Thank to Dr.Civitello in NAU for COSY spectrum.

A novel biscalixarene with two kinds of calix[4]arene derivative units connected by four bridging chains, was facilely synthesized by "1+1" condensation mode in high yield. The element analyses, ESI-MS, ¹H NMR and ¹H-¹H COSY spectrum showed that the calix[4]arene units of compound 4 were in cone conformations and compound 4 possessed biscalixarene-tube structure.
- Biscalixarene,
- Tube,
- Synthesis,
- ¹H-¹H COSY
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