引用本文:
Qi Feng Jin, Gong Xiong Liao, Xi Gao Jian. Synthesis and characterization of trimethoxysilyl-functionalized poly (phthalazinone ether ketone)[J]. Chinese Chemical Letters,
2007, 18(9): 1137-1140.
doi:
10.1016/j.cclet.2007.06.029
Citation: Qi Feng Jin, Gong Xiong Liao, Xi Gao Jian. Synthesis and characterization of trimethoxysilyl-functionalized poly (phthalazinone ether ketone)[J]. Chinese Chemical Letters, 2007, 18(9): 1137-1140. doi: 10.1016/j.cclet.2007.06.029
Citation: Qi Feng Jin, Gong Xiong Liao, Xi Gao Jian. Synthesis and characterization of trimethoxysilyl-functionalized poly (phthalazinone ether ketone)[J]. Chinese Chemical Letters, 2007, 18(9): 1137-1140. doi: 10.1016/j.cclet.2007.06.029
Synthesis and characterization of trimethoxysilyl-functionalized poly (phthalazinone ether ketone)
摘要:
A novel alkoxysilyl-functionalized poly (phthalazinone ether ketone) (PPEK) was prepared for the boundary lubricant application in micro-electro-mechanical system (MEMS). The synthesis of functionalized PPEK was started from the hydroxylation of PPEK, then following with the corresponding ring-opening reaction of 3-glycidoxypropyltrimethoxysilane (GPTMS). The structures of the functional PPEK were confirmed by FTIR, 1H NMR, 29Si NMR, and UV-vis spectrum.
English
Synthesis and characterization of trimethoxysilyl-functionalized poly (phthalazinone ether ketone)
Abstract:
A novel alkoxysilyl-functionalized poly (phthalazinone ether ketone) (PPEK) was prepared for the boundary lubricant application in micro-electro-mechanical system (MEMS). The synthesis of functionalized PPEK was started from the hydroxylation of PPEK, then following with the corresponding ring-opening reaction of 3-glycidoxypropyltrimethoxysilane (GPTMS). The structures of the functional PPEK were confirmed by FTIR, 1H NMR, 29Si NMR, and UV-vis spectrum.
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Key words:
- Phthalazinone
- / Poly (aryl ether ketone)
- / Glycidoxypropyltrimethoxysilane
- / Synthesis
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