引用本文:
Jian Jun Li, Shu Hui Jin, Xiao Mei Liang, De Kai Yuan, Dao Quan Wang. Synthesis of 12-alkoxycarbonylmethylene-1, 15-pentadecanolides[J]. Chinese Chemical Letters,
2007, 18(8): 915-916.
doi:
10.1016/j.cclet.2007.05.042
Citation: Jian Jun Li, Shu Hui Jin, Xiao Mei Liang, De Kai Yuan, Dao Quan Wang. Synthesis of 12-alkoxycarbonylmethylene-1, 15-pentadecanolides[J]. Chinese Chemical Letters, 2007, 18(8): 915-916. doi: 10.1016/j.cclet.2007.05.042
Citation: Jian Jun Li, Shu Hui Jin, Xiao Mei Liang, De Kai Yuan, Dao Quan Wang. Synthesis of 12-alkoxycarbonylmethylene-1, 15-pentadecanolides[J]. Chinese Chemical Letters, 2007, 18(8): 915-916. doi: 10.1016/j.cclet.2007.05.042
Synthesis of 12-alkoxycarbonylmethylene-1, 15-pentadecanolides
摘要:
Six novel 12-alkoxycarbonylmethylene-1, 15-pentadecanolides (3) were synthesized from 2-nitrocyclo-dodecanone by the Michael addition with acrolein followed by ring enlargement, Nef reaction and Wittig-Horner reaction. Their structures were confirmed by 1H NMR, IR and elemental analysis. The preliminary bioassay showed that they have some fungicidal activity.
English
Synthesis of 12-alkoxycarbonylmethylene-1, 15-pentadecanolides
Abstract:
Six novel 12-alkoxycarbonylmethylene-1, 15-pentadecanolides (3) were synthesized from 2-nitrocyclo-dodecanone by the Michael addition with acrolein followed by ring enlargement, Nef reaction and Wittig-Horner reaction. Their structures were confirmed by 1H NMR, IR and elemental analysis. The preliminary bioassay showed that they have some fungicidal activity.
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