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TCF/Co@NC复合纳米纤维的可控制备及其微波吸收性能

石章琳 ,  修涛 ,  毛新蒙 ,  吴建锋 ,  张宝亮

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引用本文: 石章琳, 修涛, 毛新蒙, 吴建锋, 张宝亮. TCF/Co@NC复合纳米纤维的可控制备及其微波吸收性能[J]. 物理化学学报, 2026, 42(11): 100306. doi: 10.1016/j.actphy.2026.100306 shu
Citation:  Zhanglin Shi,  Tao Xiu,  Xinmeng Mao,  Jianfeng Wu,  Baoliang Zhang. TCF/Co@NC复合纳米纤维的可控制备及其微波吸收性能[J]. Acta Physico-Chimica Sinica, 2026, 42(11): 100306. doi: 10.1016/j.actphy.2026.100306 shu

TCF/Co@NC复合纳米纤维的可控制备及其微波吸收性能

  • 1.

    西北工业大学化学与化工学院, 陕西 西安 710072;

  • 2.

    西北工业大学西安功能有机多孔材料重点实验室, 陕西 西安 710072;

  • 3.

    蓝晓科技新材料股份有限公司陕西功能高分子吸附分离工程技术研究中心, 陕西 西安 710076

    • 通讯作者: 张宝亮,E-mail:blzhang@nwpu.edu.cn
  • 基金项目:

    本研究由国家自然科学基金(22375166)；陕西省自然科学基础研究计划(2024JC-JCQN-44)及陕西省创新能力支撑计划-科技创新团队项目(2025RS-CXTD-024)资助

摘要: 将磁性纳米颗粒复合到一维(1D)多孔碳基质上具有重要研究价值。该策略对于制备高效且功能协同的微波吸收体至关重要。本工作通过超交联聚合从管状多孔纤维衍生出一维碳材料，以此为前驱体构建了一系列涂覆Co/Zn金属有机框架(MOFs)的复合纤维(C-CCNFs@Co/Zn-MOFs)。优化了包覆工艺，揭示了Zn2+离子对MOF晶粒尺寸的调控机制。后续碳化处理获得磁性氮掺杂碳包覆钴/管状碳纳米纤维(TCF/Co@NC)。该TCF/Co@NC具有多孔核壳结构和一维形貌，富含异质界面。这些特性有利于构建导电损耗网络并产生多重反射，形成强能量耗散能力。通过调节Co/Zn摩尔比，可优化复合纤维的电磁参数，从而调控其微波吸收性能。所制备的NCT-3 (Co/Zn=1 : 1)在2.7 mm厚度处获得-55.5 dB的最小反射损耗(RLmin)；而NCT-2 (Co/Zn=3 : 1)在2.4 mm厚度下展现出7.3 GHz的有效吸收带宽(EAB)。本研究为设计高性能磁性碳基微波吸收材料提供了普适且可借鉴的方法论。

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