界面工程II型异质结ZnIn2S4/SCN用于增强纯水中光催化H2O2合成

引用本文: 权永康, 李瑞东, 阳云飞, 丁述国, 陈榕兴, 黄剑莹, 吴永豪, 赖跃坤. 界面工程II型异质结ZnIn₂S₄/SCN用于增强纯水中光催化H₂O₂合成[J]. 物理化学学报, 2026, 42(10): 100237. doi: 10.1016/j.actphy.2026.100237 shu

Citation: Yongkang Quan, Ruidong Li, Yunfei Yang, Shuguo Ding, Rongxing Chen, Jianying Huang, Yun Hau Ng, Yuekun Lai. Interface engineered Type-II heterojunction ZnIn₂S₄/SCN for enhanced photocatalytic H₂O₂ synthesis from pure water[J]. Acta Physico-Chimica Sinica, 2026, 42(10): 100237. doi: 10.1016/j.actphy.2026.100237 shu

界面工程II型异质结ZnIn₂S₄/SCN用于增强纯水中光催化H₂O₂合成

权永康 ^1,2, ,
李瑞东 ^4, ,
阳云飞 ^1, ,
丁述国 ^1, ,
陈榕兴 ^1, ,
黄剑莹 ^{1,
,} ,
吴永豪 ^{5,6,
,} ,
赖跃坤 ^{1,2,3,
,}

1.
福州大学化学工程学院, 福建福州 350116;
2.
清源创新实验室, 福建泉州 362801;
3.
武汉纺织大学新型纺织材料与先进加工省重点实验室, 湖北武汉 430073;
4.
西北大学化工学院, 陕西西安 710069;
5.
香港城市大学能源与环境学院, 香港九龙塘 999077;
6.
Center for Renewable Energy and Storage Technologies (CREST), Physical Science and Engineering (PSE) Division, King Abdullah University of Science and Technology (KAUST), Thuwal 23955-6900, Saudi Arabia

通讯作者: 黄剑莹,E-mail:jyhuang@fzu.edu.cn; 吴永豪,E-mail:yunhau.ng@cityu.edu.hk; 赖跃坤,E-mail:yklai@fzu.edu.cn

基金项目:
国家自然科学基金国际(地区)合作与交流项目(22361162607)；国家自然科学基金(22375047, 22378068)；国家重点研发计划(2022YFB3804905, 2022YFB3804900)；福建省自然科学基金(2022J01568)；陕西省自然科学基础研究计划(2024JC-JCQN-19)；中国博士后科学基金(2024M752618)

摘要: 过氧化氢(H₂O₂)作为一种绿色化学品被广泛应用于众多工业领域。光催化合成H₂O₂是一种前景广阔的绿色合成路径。然而，单一半导体材料受限于光生电荷分离不足和光催化反应效率低下等问题。构建异质结以增强界面电子转移、改善电荷分离，对提升光催化活性至关重要。本研究采用两步法构建了II型异质结ZnIn₂S₄/SCN，形成了定向高速的e^-/h⁺传输通道。内置电场(BEF)为界面处的e^-/h⁺传输与分离提供了驱动力。得益于精心设计的界面结构，单一半导体光催化剂中光生电子-空穴对的高复合率及其较低的光催化活性问题得到了有效解决。ZnIn₂S₄/SCN异质结在纯水介质中通过氧还原反应(ORR)机制，在空气条件下实现257.0 μmol g^-1 h^-1的过氧化氢产率，实现了高效的光催化H₂O₂合成。本研究基于异质结设计，为高效光催化合成H₂O₂提供了重要参考。

关键词:

English

Interface engineered Type-II heterojunction ZnIn₂S₄/SCN for enhanced photocatalytic H₂O₂ synthesis from pure water

1.
College of Chemical Engineering, Fuzhou University, Fuzhou 350116, Fujian Province, China;
2.
Qingyuan Innovation Laboratory, Quanzhou 362801, Fujian Province, China;
3.
State Key Laboratory of New Textile Materials and Advanced Processing, Wuhan Textile University, Wuhan 430073, Hubei Province, China;
4.
School of Chemical Engineering, Northwest University, Xi'an 710069, Shaanxi Province, China;
5.
School of Energy and Environment, City University of Hong Kong, Kowloon Tong 999077, Hong Kong, China;
6.
Center for Renewable Energy and Storage Technologies (CREST), Physical Science and Engineering (PSE) Division, King Abdullah University of Science and Technology (KAUST), Thuwal 23955-6900, Saudi Arabia

Corresponding author: Jianying Huang, ; Yun Hau Ng, ; Yuekun Lai,

Received Date: 18 November 2025
Accepted Date: 03 January 2026
Revised Date: 02 January 2026

Abstract: Hydrogen peroxide (H₂O₂) is widely utilised as a green chemical across numerous industries. Photocatalytic synthesis of H₂O₂ represents a highly promising green synthetic pathway. However, the application of single semiconductors is constrained by limitations in photogenerated charge separation and low photocatalytic reaction efficiency. Constructing heterojunctions to enhance interfacial electron transfer and improve charge separation is crucial for enhancing photocatalytic activity. Here, a two-step approach is employed to construct a Type-II heterojunction ZnIn₂S₄/SCN, forming a directional and high-speed e^-/h⁺ transport channel. The built-in electric field (BEF) provides the driving force for the transport and separation of e^-/h⁺ at the interface. Thanks to a well-designed interface, the high recombination rate of photo-generated electron-hole pairs within a single photocatalyst and its relatively low photocatalytic activity have been effectively overcome. The ZnIn₂S₄/SCN heterojunction achieves a hydrogen peroxide yield of 257.0 μmol g^-1 h^-1 under air conditions via the oxygen reduction reaction (ORR) mechanism in pure water medium, realising highly efficient photocatalytic H₂O₂ synthesis. Based on a heterojunction design, this study provides an important reference for the highly efficient photocatalytic synthesis of hydrogen peroxide.

Key words:

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沈阳化工大学材料科学与工程学院沈阳 110142

界面工程II型异质结ZnIn₂S₄/SCN用于增强纯水中光催化H₂O₂合成

通讯作者: 黄剑莹,E-mail:jyhuang@fzu.edu.cn; 吴永豪,E-mail:yunhau.ng@cityu.edu.hk; 赖跃坤,E-mail:yklai@fzu.edu.cn

English

Interface engineered Type-II heterojunction ZnIn₂S₄/SCN for enhanced photocatalytic H₂O₂ synthesis from pure water

Corresponding author: Jianying Huang, ; Yun Hau Ng, ; Yuekun Lai,

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