MOF衍生的g-C3N4/ZnIn2S4 S型异质结：界面工程增强光催化NO转化

引用本文: 邱艳平, 张佳桐, 李林萍, 高旸钦, 李宁, 戈磊. MOF衍生的g-C₃N₄/ZnIn₂S₄ S型异质结：界面工程增强光催化NO转化[J]. 物理化学学报, 2026, 42(4): 100175. doi: 10.1016/j.actphy.2025.100175 shu

Citation: Yanping Qiu, Jiatong Zhang, Linping Li, Yangqin Gao, Ning Li, Lei Ge. MOF-derived g-C₃N₄/ZnIn₂S₄ S-scheme heterojunction: interface-engineering enhanced photocatalytic NO conversion[J]. Acta Physico-Chimica Sinica, 2026, 42(4): 100175. doi: 10.1016/j.actphy.2025.100175 shu

MOF衍生的g-C₃N₄/ZnIn₂S₄ S型异质结：界面工程增强光催化NO转化

邱艳平 ^1, ,
张佳桐 ^1, ,
李林萍 ^1, ,
高旸钦 ^1, ,
李宁 ^{1, 2,
,} ,
戈磊 ^{1, 2,
,}

1.
中国石油大学(北京)新能源与材料学院, 重质油国家重点实验室, 北京 102249
2.
中国山东省东营市利津县循环经济产业园, 东营国安化工有限公司, 山东东营 257400

通讯作者: wubian.good@163.com (李宁); Email: gelei08@sina.com (戈磊)

摘要: 为应对大气中日益严峻的氮氧化物(NO_x)污染问题，亟需开发兼具高效性与高选择性的光催化剂。本研究构建了g-C₃N₄/ZnIn₂S₄ (CN/ZIS) S型异质结光催化剂，其中通过MOF衍生策略合成了具有中空管状形貌的ZnIn₂S₄，g-C₃N₄则作为高效电子转移平台。优化后的CN/ZIS-0.1在可见光照射下表现出显著提升的光催化性能，NO去除效率达67.29%，显著高于原始g-C₃N₄ (41.41%)和ZIS (27.8%)；同时NO向硝酸盐的选择性转化率达到77.47%，亦明显优于g-C₃N₄ (49.01%)。材料表征结果表明，CN/ZIS-0.1不仅有更宽的光吸收范围，其独特结构还提供了更多反应位点。光电化学测试与DFT计算进一步证实，CN/ZIS界面形成的内建电场(BIEF)驱动光生电子向g-C₃N₄表面迁移、空穴向ZIS表面定向迁移，从而促进关键活性物种生成并增强NO吸附。本工作不仅证明了MOF衍生中空结构与二维半导体耦合构建S型异质结在NO光催化氧化中的潜力，还为开发高选择性NO光催化剂提供有效策略。

关键词:

English

MOF-derived g-C₃N₄/ZnIn₂S₄ S-scheme heterojunction: interface-engineering enhanced photocatalytic NO conversion

1.
State Key Laboratory of Heavy Oil Processing, College of New Energy and Materials, China University of Petroleum Beijing, Beijing 102249, China
2.
Dongying Guoan Chemical Co., Ltd, Circular Economy Industrial Park, Lijin County, Dongying 257400, Shandong Province, China

Corresponding author: wubian.good@163.com (Li Ning); Email: gelei08@sina.com (Ge Lei)

Received Date: 19 July 2025
Accepted Date: 25 August 2025
Revised Date: 22 August 2025
Available Online: 15 April 2026

Abstract: Addressing the growing challenge of nitrogen oxides (NO_x) pollution in the atmosphere requires the development of photocatalysts with both high efficiency and strong selectivity. In this study, a g-C₃N₄/ZnIn₂S₄ (CN/ZIS) S-scheme heterojunction photocatalyst was constructed, in which ZnIn₂S₄ with a hollow tubular morphology was synthesized via a MOF-derived strategy, and g-C₃N₄ served as an efficient electron transfer platform. The optimized CN/ZIS-0.1 exhibited remarkable photocatalytic efficacy under visible-light radiation, attaining a NO removal efficiency of 67.29%, markedly surpassing that of pristine g-C₃N₄ (41.41%) and ZIS (27.8%). Additionally, a high NO-to-nitrate selectivity of 77.47% was attained, exceeding that of pristine g-C₃N₄ (49.01%). The material characterization results revealed that CN/ZIS-0.1 not only has a wider light absorption range but also its unique structure provides more reaction sites. Further photoelectrochemical measurements and DFT simulations confirm that the built-in electric field (BIEF) formed at the CN/ZIS interface facilitates the directional migration of photogenerated electrons towards the g-C₃N₄ surface, and photogenerated holes migrate towards the surface of ZIS, thereby promoting the generation of key reactive species and enhancing NO adsorption. This work not only demonstrates the potential of constructing S-scheme heterojunctions by coupling MOF-derived hollow structures with two-dimensional semiconductors for NO oxidation, but also offers an effective strategy for developing highly selective NO photocatalysts.

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沈阳化工大学材料科学与工程学院沈阳 110142

MOF衍生的g-C₃N₄/ZnIn₂S₄ S型异质结：界面工程增强光催化NO转化

通讯作者: wubian.good@163.com (李宁); Email: gelei08@sina.com (戈磊)

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MOF-derived g-C₃N₄/ZnIn₂S₄ S-scheme heterojunction: interface-engineering enhanced photocatalytic NO conversion

Corresponding author: wubian.good@163.com (Li Ning); Email: gelei08@sina.com (Ge Lei)

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