S型异质结In2O3/ZnIn2S4光催化5-羟甲基糠醛选择性氧化耦合产氢

引用本文: 骆泽, 朱玉坤, 罗雅丹, 任广敏, 王永红, 唐华. S型异质结In₂O₃/ZnIn₂S₄光催化5-羟甲基糠醛选择性氧化耦合产氢[J]. 物理化学学报, 2026, 42(3): 100166. doi: 10.1016/j.actphy.2025.100166 shu

Citation: Ze Luo, Yukun Zhu, Yadan Luo, Guangmin Ren, Yonghong Wang, Hua Tang. Photocatalytic selective oxidation of 5-hydroxymethylfurfural coupled with H₂ evolution over In₂O₃/ZnIn₂S₄ S-scheme heterojunction[J]. Acta Physico-Chimica Sinica, 2026, 42(3): 100166. doi: 10.1016/j.actphy.2025.100166 shu

S型异质结In₂O₃/ZnIn₂S₄光催化5-羟甲基糠醛选择性氧化耦合产氢

骆泽 ^1, ,
朱玉坤 ^1, ,
罗雅丹 ^1, ,
任广敏 ^2, ,
王永红 ^1, ,
唐华 ^{1,
,}

1.
青岛大学, 环境与地理科学学院, 材料科学与工程学院, 山东青岛 266071
2.
青岛科技大学, 化工学院, 山东青岛 266042

通讯作者: Email: huatang79@163.com (唐华)

摘要: 发展可持续的光催化技术，以实现生物质向高附加值化学品和清洁燃料的高效转化，是应对全球能源与环境危机有效途径。本研究通过原位生长法构建了一种新型一维/二维(1D/2D)In₂O₃/ZnIn₂S₄ S型异质结光催化剂。该设计巧妙结合棒状In₂O₃与片状ZnIn₂S₄，促进定向电荷传输并提供高密度活性位点。因此，优化后的In₂O₃/ZnIn₂S₄异质结在420 nm LED光照下对5-羟甲基糠醛(HMF)转化率达81.6%，且对2,5-二甲酰基呋喃(DFF)和2,5-呋喃二甲酸(FDCA)的选择性高达78.2%。同时，该异质结表现出257.69 μmol g⁻¹ h⁻¹的产氢(H₂)速率。这些结果表明，S型异质结能有效实现空间电荷分离并提升光催化活性，为太阳能驱动的生物质增值与可持续产氢提供了可行策略。

关键词:

English

Photocatalytic selective oxidation of 5-hydroxymethylfurfural coupled with H₂ evolution over In₂O₃/ZnIn₂S₄ S-scheme heterojunction

Ze Luo ^1, ,
Yukun Zhu ^1, ,
Yadan Luo ^1, ,
Guangmin Ren ^2, ,
Yonghong Wang ^1, ,
Hua Tang ^{1,
,}

1.
School of Environment and Geography, College of Materials Science and Engineering, Qingdao University, Qingdao 266071, Shandong Province, China
2.
College of Chemical Engineering, Qingdao University of Science & Technology, Qingdao, 266042, Shandong Province, China

Corresponding author: Email: huatang79@163.com (Hua Tang)

Received Date: 16 July 2025
Accepted Date: 17 August 2025
Revised Date: 15 August 2025
Available Online: 15 March 2026

Abstract: Addressing the global energy and environmental crisis necessitates the development of sustainable photocatalytic technologies capable of efficiently converting biomass into high-value chemicals and clean fuels. In this study, we develop a novel one-dimensional/two-dimensional (1D/2D) In₂O₃/ZnIn₂S₄ S-scheme heterojunction photocatalyst through in situ growth process. This rationally designed architecture combines rod-like In₂O₃ with sheet-like ZnIn₂S₄ nanosheets, facilitating directional charge transport and providing a high density of active sites. Consequently, the optimized In₂O₃/ZnIn₂S₄ heterojunction achieved a 5-hydroxymethylfurfural (HMF) conversion rate of 81.6% with a high selectivity of 78.2% toward 2,5-diformylfuran (DFF) and 2,5-furandicarboxylic acid (FDCA). Furthermore, it exhibited a hydrogen (H₂) evolution rate of 257.69 μmol g⁻¹ h⁻¹ under 420 nm LED irradiation. These results demonstrate the efficacy of S-scheme heterojunctions in enabling spatial charge separation and boosting photocatalytic activity, offering a promising strategy for solar-driven biomass valorization and sustainable H₂ production.

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沈阳化工大学材料科学与工程学院沈阳 110142

S型异质结In₂O₃/ZnIn₂S₄光催化5-羟甲基糠醛选择性氧化耦合产氢

通讯作者: Email: huatang79@163.com (唐华)

English

Photocatalytic selective oxidation of 5-hydroxymethylfurfural coupled with H₂ evolution over In₂O₃/ZnIn₂S₄ S-scheme heterojunction

Corresponding author: Email: huatang79@163.com (Hua Tang)

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