Citation: Shenhui Li, Lei Zhou, Anmin Zheng, Feng Deng. Recent advances in solid state NMR characterization of zeolites[J]. Chinese Journal of Catalysis, ;2015, 36(6): 789-796. doi: 10.1016/S1872-2067(14)60290-4 shu

Recent advances in solid state NMR characterization of zeolites

1.
National Center for Magnetic Resonance in Wuhan, State Key Laboratory of Magnetic Resonance and Atomic and Molecular Physics, Wuhan Institute of Physics and Mathematics, Chinese Academy of Sciences, Wuhan 430071, Hubei, China

Corresponding author: Feng Deng,
Received Date: 7 November 2014
Available Online: 11 December 2014
Fund Project: 国家自然科学基金(21210005, 21221064, 21373265). (21210005, 21221064, 21373265)

Zeolites are widely used as ion exchangers, adsorbents and catalysts in the chemical and petrochemical industries because of their pore structure and acidity. Solid state NMR is a powerful tool for the characterization of the topological structure, active sites (acid sites) and host-guest interaction in zeolites. Recent advances in the solid state NMR characterization of zeolites are briefly reviewed.
- Solid state NMR,
- Zeolite,
- Structure determination,
- Acid site,
- Host-guest interaction
1. [1]
  [1] Hattori H. Chem Rev, 1995, 95: 537
2. [2]
  [2] Massiot D, Messinger R J, Cadars S, Deschamps M, Montouillout V, Pellerin N, Veron E, Allix M, Florian P, Fayon F. Acc Chem Res, 2013, 46: 1975
3. [3]
  [3] Brouwer D H, Darton R J, Morris R E, Levitt M H. J Am Chem Soc, 2005, 127: 10365
4. [4]
  [4] Brouwer D H, Kristiansen P E, Fyfe C A, Levitt M H. J Am Chem Soc, 2005, 127: 542
5. [5]
  [5] Brouwer D H, Enright G D. J Am Chem Soc, 2008, 130: 3095
6. [6]
  [6] Hammond K D, Dogan F, Tompsett G A, Agarwal V, Conner W C, Grey C P Jr, Auerbach S M. J Am Chem Soc, 2008, 130: 14912
7. [7]
  [7] Cadars S, Brouwer D H, Chmelka B F. Phys Chem Chem Phys, 2009, 11: 1825
8. [8]
  [8] Zheng A M, Huang X J, Wang Q, Zhang H L, Deng F, Liu S B. Chin J Catal (郑安民, 黄信炅, 王强, 张海禄, 邓风, 刘尚斌. 催化学报), 2013, 34: 436
9. [9]
  [9] Zheng A M, Liu S B, Deng F. Solid State Nucl Magn Reson, 2013, 55-56: 12
10. [10]
  [10] Peng L M, Liu Y, Kim N J, Readman J E, Grey C P. Nat Mater, 2005, 4: 216
11. [11]
  [11] Peng L M, Huo H, Liu Y, Grey C P. J Am Chem Soc, 2007, 129: 335
12. [12]
  [12] Huo H, Peng L M, Gan Z H, Grey C P. J Am Chem Soc, 2012, 134: 9708
13. [13]
  [13] Sohn J R, DeCanio S J, Fritz P O, Lunsford J H. J Phys Chem, 1986, 90: 4847
14. [14]
  [14] Shannon R D, Gardner K H, Staley R H, Bergeret G, Gallezot P, Auroux A. J Phys Chem, 1985, 89: 4778
15. [15]
  [15] Feike M, Demco D E, Graf R, Gottwald J, Hafner S, Spiess H W. J Magn Reson A, 1996, 122: 214
16. [16]
  [16] Mali G, Taulelle F. Chem Commun, 2004: 868
17. [17]
  [17] Li S H, Zheng A M, Su Y C, Zhang H L, Chen L, Yang J, Ye C H, Deng F. J Am Chem Soc, 2007, 129: 11161
18. [18]
  [18] Li S H, Huang S J, Shen W L, Zhang H L, Fang H J, Zheng A M, Liu S B, Deng F. J Phys Chem C, 2008, 112: 14486
19. [19]
  [19] Yu Z W, Zheng A M, Wang Q, Chen L, Xu J, Amoureux J P, Deng F. Angew Chem Int Ed, 2010, 49: 8657
20. [20]
  [20] Wang Q, Hu B, Lafon O, Trebosc J, Deng F, Amoureux J P. J Magn Reson, 2009, 200: 251
21. [21]
  [21] Yu Z W, Li S H, Wang Q, Zheng A M, Xu J, Chen L, Deng F. J Phys Chem C, 2011, 115: 22320
22. [22]
  [22] Peng L M, Chupas P J, Grey C P. J Am Chem Soc, 2004, 126: 12254
23. [23]
  [23] Peng L M, Grey C P. Micropor Mesopor Mater, 2008, 116: 277
24. [24]
  [24] Wolf P, Valla M, Rossini A J, Comas-Vives A, Núñez-Zarur F, Malaman B, Lesage A, Emsley L, Copéret C, Hermans I. Angew Chem Int Ed, 2014, 53: 10179
25. [25]
  [25] Ni Q Z, Daviso E, Can T V, Markhasin E, Jawla S K, Swager T M, Temkin R J, Herzfeld J, Griffin R G. Acc Chem Res, 2013, 46: 1933
26. [26]
  [26] Rossini A J, Zagdoun A, Lelli M, Lesage A, Copéret C, Emsley L. Acc Chem Res, 2013, 46: 1942
27. [27]
  [27] Gunther W R, Michaelis V K, Caporini M A, Griffin R G, Román-Leshkov Y. J Am Chem Soc, 2014, 136: 6219
28. [28]
  [28] Fyfe C A, Brouwer D H. J Am Chem Soc, 2006, 128: 11860
29. [29]
  [29] Comotti A, Bracco S, Valsesia P, Ferretti L, Sozzani P. J Am Chem Soc, 2007, 129: 8566
30. [30]
  [30] Janicke M T, Landry C C, Christiansen S C, Kumar D, Stucky G D, Chmelka B F. J Am Chem Soc, 1998, 120: 6940
31. [31]
  [31] Christiansen S C, Zhao D Y, Janicke M T, Landry C C, Stucky G D, Chmelka B F. J Am Chem Soc, 2001, 123: 4519
32. [32]
  [32] Chen B H, Huang Y N. J Am Chem Soc, 2006, 128: 6437
33. [33]
  [33] Shen W L, Li S H, Xu J, Zhang H L, Hu W, Zhou D, Zhang J N, Yu J H, Xu W J, Xu Y, Deng F. J Phys Chem C, 2010, 114: 7076
34. [34]
  [34] Lesage A, Lelli M, Gajan D, Caporini M A, Vitzthum V, Miéville P, Alauzun J, Roussey A, Thieuleux C, Mehdi A, Bodenhausen G, Coperet C, Emsley L. J Am Chem Soc, 2010, 132: 15459
35. [35]
  [35] Lelli M, Gajan D, Lesage A, Caporini M A, Vitzthum V, Miéville P, Héroguel F, Rascón F, Roussey A, Thieuleux C, Boualleg M, Veyre L, Bodenhausen G, Coperet C, Emsley L. J Am Chem Soc, 2011, 133: 2104
36. [36]
  [36] Li S H, Deng F. Annu Rep NMR Spectrosc, 2013, 78: 1
37. [37]
  [37] Gan Z H. Chem Commun, 2006: 4712
38. [38]
  [38] Li S H, Pourpoint F, Trébosc J, Zhou L, Lafon O, Shen M, Zheng A M, Wang Q, Amoureux J P, Deng F. J Phys Chem Lett, 2014, 5: 3068
39. [39]
  [39] Xu T, Munson E J, Haw J F. J Am Chem Soc, 1994, 116: 1962
40. [40]
  [40] Pourpoint F, Trébosc J, Gauvin R M, Wang Q, Lafon O, Deng F, Amoureux J P. ChemPhysChem, 2012, 13: 3605
41. [41]
  [41] Tricot G, Lafon O, Trebosc J, Delevoye L, Mear F, Montagne L, Amoureux J P. Phys Chem Chem Phys, 2011, 13: 16786
42. [42]
  [42] Haw J F, Song W G, Marcus D M, Nicholas J B. Acc Chem Res, 2003, 36: 317
43. [43]
  [43] Wang W, Hunger M. Acc Chem Res, 2008, 41: 895
44. [44]
  [44] Chu Y Y, Han B, Zheng A M, Deng F. J Phys Chem C, 2012, 116: 12687
1. [1]
  Pei Li , Yuenan Zheng , Zhankai Liu , An-Hui Lu . Boron-Containing MFI Zeolite: Microstructure Control and Its Performance of Propane Oxidative Dehydrogenation. Acta Physico-Chimica Sinica, 2025, 41(4): 100034-. doi: 10.3866/PKU.WHXB202406012
2. [2]
  Yuxin CHEN , Yanni LING , Yuqing YAO , Keyi WANG , Linna LI , Xin ZHANG , Qin WANG , Hongdao LI , Wenmin WANG . Construction, structures, and interaction with DNA of two Sm^Ⅲ₄ complexes. Chinese Journal of Inorganic Chemistry, 2025, 41(6): 1141-1150. doi: 10.11862/CJIC.20240258
3. [3]
  Jiaxun Wu , Mingde Li , Li Dang . The R eaction of Metal Selenium Complexes with Olefins as a Tutorial Case Study for Analyzing Molecular Orbital Interaction Modes. University Chemistry, 2025, 40(3): 108-115. doi: 10.12461/PKU.DXHX202405098
4. [4]
  Hao Wu , Zhen Liu , Dachang Bai . ¹H NMR Spectrum of Amide Compounds. University Chemistry, 2024, 39(3): 231-238. doi: 10.3866/PKU.DXHX202309020
5. [5]
  Yuhao SUN , Qingzhe DONG , Lei ZHAO , Xiaodan JIANG , Hailing GUO , Xianglong MENG , Yongmei GUO . Synthesis and antibacterial properties of silver-loaded sod-based zeolite. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 761-770. doi: 10.11862/CJIC.20230169
6. [6]
  Jiali CHEN , Guoxiang ZHAO , Yayu YAN , Wanting XIA , Qiaohong LI , Jian ZHANG . Machine learning exploring the adsorption of electronic gases on zeolite molecular sieves. Chinese Journal of Inorganic Chemistry, 2025, 41(1): 155-164. doi: 10.11862/CJIC.20240408
7. [7]
  Yiping HUANG , Liqin TANG , Yufan JI , Cheng CHEN , Shuangtao LI , Jingjing HUANG , Xuechao GAO , Xuehong GU . Hollow fiber NaA zeolite membrane for deep dehydration of ethanol solvent by vapor permeation. Chinese Journal of Inorganic Chemistry, 2025, 41(2): 225-234. doi: 10.11862/CJIC.20240224
8. [8]
  Jinkang Jin , Yidian Sheng , Ping Lu , Zhan Lu . Introducing a Website for Learning Nuclear Magnetic Resonance (NMR) Spectrum Analysis. University Chemistry, 2024, 39(11): 388-396. doi: 10.12461/PKU.DXHX202403054
9. [9]
  Haolin Zhan , Qiyuan Fang , Jiawei Liu , Xiaoqi Shi , Xinyu Chen , Yuqing Huang , Zhong Chen . Noise Reduction of Nuclear Magnetic Resonance Spectroscopy Using Lightweight Deep Neural Networ. Acta Physico-Chimica Sinica, 2025, 41(2): 100017-. doi: 10.3866/PKU.WHXB202310045
10. [10]
  Haiyang Jin , Yonghai Hui , Yongfei Zhang , Lijun Gao , Yun Wang . Application and Exploration of Nuclear Magnetic Resonance Spectrometer in Undergraduate Basic Laboratory Teaching. University Chemistry, 2025, 40(3): 245-250. doi: 10.12461/PKU.DXHX202406022
11. [11]
  Yufang GAO , Nan HOU , Yaning LIANG , Ning LI , Yanting ZHANG , Zelong LI , Xiaofeng LI . Nano-thin layer MCM-22 zeolite: Synthesis and catalytic properties of trimethylbenzene isomerization reaction. Chinese Journal of Inorganic Chemistry, 2024, 40(6): 1079-1087. doi: 10.11862/CJIC.20240036
12. [12]
  Shanghua Li , Malin Li , Xiwen Chi , Xin Yin , Zhaodi Luo , Jihong Yu . 基于高离子迁移动力学的取向ZnQ分子筛保护层实现高稳定水系锌金属负极的构筑. Acta Physico-Chimica Sinica, 2025, 41(1): 2309003-. doi: 10.3866/PKU.WHXB202309003
13. [13]
  Zhuoming Liang , Ming Chen , Zhiwen Zheng , Kai Chen . Multidimensional Studies on Ketone-Enol Tautomerism of 1,3-Diketones By ¹H NMR. University Chemistry, 2024, 39(7): 361-367. doi: 10.3866/PKU.DXHX202311029
14. [14]
  Hui Wang , Abdelkader Labidi , Menghan Ren , Feroz Shaik , Chuanyi Wang . 微观结构调控的g-C₃N₄在光催化NO转化中的最新进展：吸附/活化位点的关键作用. Acta Physico-Chimica Sinica, 2025, 41(5): 100039-. doi: 10.1016/j.actphy.2024.100039
15. [15]
  Huiying Xu , Minghui Liang , Zhi Zhou , Hui Gao , Wei Yi . Application of Quantum Chemistry Computation and Visual Analysis in Teaching of Weak Interactions. University Chemistry, 2025, 40(3): 199-205. doi: 10.12461/PKU.DXHX202407011
16. [16]
  Hailian Tang , Siyuan Chen , Qiaoyun Liu , Guoyi Bai , Botao Qiao , Fei Liu . Stabilized Rh/hydroxyapatite Catalyst for Furfuryl Alcohol Hydrogenation: Application of Oxidative Strong Metal-Support Interactions in Reducing Conditions. Acta Physico-Chimica Sinica, 2025, 41(4): 100036-. doi: 10.3866/PKU.WHXB202408004
17. [17]
  Zehua Zhang , Haitao Yu , Yanyu Qi . 多重共振TADF分子的设计策略. Acta Physico-Chimica Sinica, 2025, 41(1): 2309042-. doi: 10.3866/PKU.WHXB202309042
18. [18]
  Wenjie SHI , Fan LU , Mengwei CHEN , Jin WANG , Yingfeng HAN . Synthesis and host-guest properties of imidazolium-functionalized zirconium metal-organic cage. Chinese Journal of Inorganic Chemistry, 2025, 41(1): 105-113. doi: 10.11862/CJIC.20240360
19. [19]
  Wen-Bing Hu . Systematic Introduction of Polymer Chain Structures. University Chemistry, 2025, 40(4): 15-19. doi: 10.3866/PKU.DXHX202401014
20. [20]
  Kai Yang , Gehua Bi , Yong Zhang , Delin Jin , Ziwei Xu , Qian Wang , Lingbao Xing . Comprehensive Polymer Chemistry Experiment Design: Preparation and Characterization of Rigid Polyurethane Foam Materials. University Chemistry, 2024, 39(4): 206-212. doi: 10.3866/PKU.DXHX202308045

Get Citation

PDF

XML

Metrics

PDF Downloads(2)
Abstract views(419)
HTML views(33)

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142