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Yang Chuncai, Jing Xiabin, Wang Huabin, Chen Tianlu, Han Xiaozu, Wang Fosong. Synthesis and Poling of A Crosslinked Second Order Nonlinear Optical Polymer with Liquid Crystalline Side Groups[J]. Chinese Journal of Applied Chemistry,
;1995, 12(4): 7-12.
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The synthesis of glycerin monoether of 4-[(p-nitrophenyl) azoxy] phenol which can form liquid crystalline phases is reported. The crosslinking reaction of glycerin mo-noether of 4-[(p-nitrophenyl) azoxy] phenol by biuret of hexamethylene diisocyanate has been studied by DSC and FTIR spectra. The orientation and stability of a poled and crosslinked polymer have been investigated by UV-Vis spectra. The orientation relaxation was not observed in 100 hours for the poled and crosslinked polymer after poling and crosslinking for 1h at 150℃.
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