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Citation: Sheng Shouri, Cai Mingzhong, Song Caisheng. Synthesis and Characterization of Poly(aryl Ether Sulfone Ether Ketone Ketone) Containing Naphthalene Links[J]. Chinese Journal of Applied Chemistry, ;1998, 15(5): 47-49. shu

Synthesis and Characterization of Poly(aryl Ether Sulfone Ether Ketone Ketone) Containing Naphthalene Links

Department of Chemistry, Jiangxi Normal University, Nanchang 330027

Received Date: 23 November 1997
Revised Date: 24 April 1998

4,4'-bis(U-naphthoxy)diphenylsulfone(BNODPS) was synthesized by reaction of U-naphthol with bis(4-chlorophenyl) sulfone in DMSO in the presence of KOH. Five polyaryl ether sulfone ether ketone ketones containing naphthalene links were prepared by low temperature solution polycondensation of BNODPS with terephthaloyl chloride(TPC), isophthaloyl chloride(IPC) and 2,5-dichloroterephthaloyl chloride(DCC), respectively in 1,2-dichlorothane and in the presence of AlCl₃ and N-methylpyrrolidone. The polymers as characterized by IR, XRD, DSC and TG techniques are non-crystalline and have high glass transition temperature, good thermostability and solubitity.
- polyaryl ether sulfone ether ketone ketone,
- synthesis,
- U-naphthol,
- aromatic diacid chloride,
- low temperature solution polycondensation
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