Citation: Li Haiying, Liu Zheng, Guo Yajin, Guo Peng, Lao Xinqiao, Zhang Shufen. Syntheses, Characterizations and Properties of 4-Formyl-benzoic acid adamantan-1-yl ester Schiff Base and Their Ni(Ⅱ) Complexes[J]. Chemistry, ;2017, 80(8): 765-771. shu

Syntheses, Characterizations and Properties of 4-Formyl-benzoic acid adamantan-1-yl ester Schiff Base and Their Ni(Ⅱ) Complexes

College of Chemical and Biological Engineering, Guilin University of Technology; Guangxi Key Laboratory of Electrochemical and Magneto-chemical Functional Materials, Guilin 541004

Corresponding author: Liu Zheng, lisa4.6@163.com
Received Date: 21 October 2016
Accepted Date: 4 March 2017

Figures(5)

Three different Schiff bases containing adamantanyl ester of formyl benzoic acid and their Ni(Ⅱ) complexes were synthesized using adamantanol, 4-formylbenzoic acid, o-aminophenal, 2-aminothiophenol and 2-bromoaniline as raw materials. Their structures were characterized by IR, UV-Vis and NMR spectroscopies. The fluorescence properties, thermal stabilities and electrochemical properties of Schiff bases and their Ni(Ⅱ) complexes were studied through fluorescence spectra, thermogravimetric analysis and electrochemical techniques. The results indicated that Ni(Ⅱ) complexes H1, H2 and H3 have good fluorescence properties and H1, H2 exhibit high electrochemical activity.
- Adamantanol,
- Schiff base,
- Ni(Ⅱ) complexes,
- Fluorescence property,
- Electrochemical activity
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