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Citation: Wang Yang, Wang Qiaochun. Synthesis of Perhydroxycucurbi[6] turil Based on K₂S₂O₈-KOH System[J]. Chemistry, ;2018, 81(4): 376-379. shu

Synthesis of Perhydroxycucurbi[6] turil Based on K₂S₂O₈-KOH System

Wang Yang ,
Wang Qiaochun ^,

Key Laboratory for Advanced Materials and Institute of Fine Chemicals, School of Chemistry & Molecular Engineering, East China University of Science & Technology, Shanghai 200237

Corresponding author: Wang Qiaochun, qcwang@ecust.edu.cn
Received Date: 21 November 2017
Accepted Date: 10 January 2018

Figures(3)

Based on the reported synthesis of perhydroxycucurbi[6]turil with cucurbituril-potassium persulfate system, the effect of adding KOH to the original system has been studied. Under the optimized reaction conditions, the desired product can be obtained in satisfactory yield (27%). The product was further identified by the ¹H NMR, ¹³C NMR and HR-ESI-MS.
- Perhydroxycucurbi[6]turils,
- KPS,
- KOH,
- Synthesis
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Synthesis of Perhydroxycucurbi[6] turil Based on K₂S₂O₈-KOH System