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Citation: Huang Xiwen, Zhen Hanfei, Wang Shulan, Cong Peijun, Wang Rongshu. Synthesis of Mesopore Molecular Sieve Embedded with Synergistic Extrant[J]. Chinese Journal of Applied Chemistry, ;1997, 14(6): 30-33. shu

Synthesis of Mesopore Molecular Sieve Embedded with Synergistic Extrant

1.
Department of Chemical Engineering, Tianjin University, Tianjin 300072

Received Date: 13 May 1997
Available Online: 3 September 1997
Fund Project:

The liquid crystalline phase micell formed from cetyltrimethylammonium hydro-xide was used as template with simultaneous introduction of a synergistic extractant TOPO-D₂EPHA into it. A mesoporous molecular sieve embedded with synergistic extractant MCM-TP was obtained. It is formed through the self-assembly process between the hydrophilic groups of the micell and organic silicate anions. The results from TEM, XRD, and ²⁹Si-MASNMR showed that the sieve had a similar hexagonal arrangement of uniform mesopores as that of MCM-41, but an improved hydrothermal stability with saturation adsorption of 0.015 mmol[Pd]/g.
- spent nuclear fuel,
- palladium extraction,
- mesopore molecular sieve,
- synergistic extractant
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