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Citation: Din Yanbin, Fan Ailong, Zhang Zheng. Synthesis of 2-( Arylsulfonyl)-1-( 2-thienyl) ethanone[J]. Chinese Journal of Applied Chemistry, ;1997, 14(3): 113-114. shu

Synthesis of 2-( Arylsulfonyl)-1-( 2-thienyl) ethanone

1.
Department of Chemistry, Nanjing University, Nanjing 210093

Received Date: 12 August 1996
Available Online: 13 January 1997

A series of 2-(4-R-phenylsulfonyl)-1-(2-thienyl) ethanone( R=H, CH₃, F, Cl, Br) were prepared in 75%~96% yields by reaction of sodium arylsulfinate with 2-chloro-1-(2-thienyl) ethanone in the presence of triethyl benzylam monium ohldride at 80~85℃.Their structures were confirm ed by elemental analysis, IR and ¹H NMR.
- chlorothienylethanone,
- arylsulfonylthienylethanone,
- synthesis,
- phase transfer catalysis
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