Citation:
Li Duxin, Chen Liang, Gao Xiaoyan. AN IMPROVED METHOD FOR PREPARATION OF TETRAPHENYLPORPHYRIN[J]. Chinese Journal of Applied Chemistry,
;1993, 10(5): 95-96.
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The method of preparation of tetraphenylporphyrin (H2TPP) has been improved by using a mixed solvent based on the propionic acid and thionyl chloride as oxidizing agent instead of 2, 3-dichloro-5,6-dicyanobenzoqinone. The yield of the pure H2TPP achieved 38%. Six complexes of H2TPP with Cu, Co, Ni, Fe, In, and La were prepared respectively.
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Keywords:
- tetraphenylporphyrin,
- porphyrin metal complex,
- preparation
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