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Citation: Feng Xiaoming, Chen Rong, Zhang Ziyi. SYNTHESIS OF 1-PHENYLACETYL-4-AROYLTHIOSEMICAR-BAZIDES AND THEIR CYCLIZATION[J]. Chinese Journal of Applied Chemistry, ;1993, 10(1): 104-106. shu

SYNTHESIS OF 1-PHENYLACETYL-4-AROYLTHIOSEMICAR-BAZIDES AND THEIR CYCLIZATION

1.
1. Department of Chemistry, Southwest Normal University, 630715 Chongqing;
2.
2. Department of Chemistry, Lanzhou University, Lanzhou

Received Date: 27 January 1992
Available Online: 25 June 1992

A series of 1-phenylaeetyl-4-aroylthiosemicarbazides (1) were synthesized by the reaction of phenylacetylhydrazine with aroyl isothiocyanates. Some of 3-benzyl-4-aroyl-1,2, 4-triazoline-5-thione (2) were obtained in good yields through the cyclization of 1 in 1mol/LK₂CO₃ solution. The structures of all compounds prepared were characterized by elemental analysis,IR,¹H NMR and MS.The preliminary experiments showed that compounds 1 and 2 possess some inhibiting activity on B. substilis.
- acylthiosemicarbazide,
- triazolinethione,
- synthesis,
- bactericide
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