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Citation: ZHANG Hong-Bo, WANG Yi-Min, JIANG Jing, CUI Guang, ZHAO Lei, SHAO Jing, SU Chun-Hui. Preparation and Characterization of Neodymium-Doped Phosphate Glass-Ceramic[J]. Chinese Journal of Applied Chemistry, ;2009, 26(8): 948-951. shu

Preparation and Characterization of Neodymium-Doped Phosphate Glass-Ceramic

ZHANG Hong-Bo ^a ,
WANG Yi-Min ^c ,
JIANG Jing ^a ,
CUI Guang ^a ,
ZHAO Lei ^a ,
SHAO Jing ^a ,
SU Chun-Hui ^a,b,,

1.
a College of Chemical and Environmental Engineering, Changchun University of Science and Technology, Changchun 130022;
2.
b Jilin Teacher's Institute of Engineering and Technology, Changchun;
3.
c Jilin Vocational College of Industry and Technology, Jilin

Corresponding author: SU Chun-Hui,
Received Date: 28 July 2008
Available Online: 23 October 2008
Fund Project: 教育部科学技术重点项目(205037) (205037)教育部博士点基金项目(20050186004) (20050186004)

The transparent neodymium-doped phosphate glass-ceramic was prepared by the method of melting and crystallization.The obtained glas-ceramic was characterized by DTA,XRD,SEM,UV-Vis-NIR and fluorescence spectrometry.The results indicate that the main crystal phase of the transparent glass-ceramic is Al₂SiO₅.The temperature of nuclear generation is in a range from 490~540 ℃,and the time of treatment is about 1~2 h.The temperature of crystallization is at 550 ℃,and the time of treatment is about 1~3 h.The average grain size is 90 nm.The transparency of the glass-ceramic can reach to 69%,which decreases with the incerease of the heat-treatment time.Because of the concentration increase of Nd³⁺ in the crystal phase after the heat treatment,the peak of the glass-ceramic is stronger than the host glass at 1 056 nm in fluore-scence spectra.
- melting method,
- phosphate,
- glass-ceramics,
- neodymium-doped
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