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Citation: WANG Zhen-Hui, HUANG Ai-Ping, QIAO Hai-Yan, CHEN Ti-Wei, WANG Dong. Fabrication of Inlaid Super-thin Microcrystalline Cellulose Modified Carbon Paste Film Electrode and Its Application[J]. Chinese Journal of Applied Chemistry, ;2009, 26(7): 840-844. shu

Fabrication of Inlaid Super-thin Microcrystalline Cellulose Modified Carbon Paste Film Electrode and Its Application

1.
College of Chemistry and Environmental Science, Henan Normal University, Xinxiang 453007

Corresponding author: WANG Zhen-Hui,
Received Date: 3 July 2008
Available Online: 9 September 2008
Fund Project: 国家自然科学基金资助项目(20675026) (20675026)

A novel inlaid super-thin microcrystalline cellulose modified carbon paste film electrode(ISM/CPE) was fabricated by direct inlaying microcrystalline cellulose modified carbon paste film on the surface of nichrome substrate.The characteristics of ISM/CPE were investigated by scanning electron microscopy(SEM) and cyclic voltammetry.The electrochemical behavior of the electrode was examined with ascorbic acid(AA) as an object.The oxidation peak potential(E_pa) of AA was observed at 0.38 V,which was shifted by 0.05 V negatively compared to the E_pa at the conventional carbon paste electrode.The oxidation peak current was linearly proportional to the concentration of AA in a range of 1.0×10^-6～1.0×10^-3 mol/L with a correlation coefficient of 0.999 3 and a detection limit(S/N=3) of 7.5×10^-7 mol/L,showing that the electrochemical properties of the substrate electrode were changed after super-thin microcrystalline cellulose modified carbon paste film was inlaid and it could be applied to the determination of AA in real samples.
- microcrystalline cellulose,
- inlaid super-thin carbon paste film,
- Voltammetry,
- ascorbic acid
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