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Citation: HUO Li-Hua, WANG Xu, ZHAO Jing-Gui, MA Shu-Jie. Synthesis and Characterization of Metal Titanate Zeolites[J]. Chinese Journal of Applied Chemistry, ;2000, 17(3): 322-324. shu

Synthesis and Characterization of Metal Titanate Zeolites

a.
a. College of Chemistry and Chemical Technology, Heilongjiang University, Harbin 150080;
b.
b. Department of Chemistry, Jilin University, Changchun

Received Date: 12 October 1999
Available Online: 17 January 2000
Fund Project: 黑龙江省自然科学基金资助项目(9732) (9732)

Cobalt titanate and gallium titanate zeolites were synthesized hydrothermally using tetraethylammonium hydroxide and/or tetrapropylammonium bromide as template. The study of the effects of pH value, amount and feed order of template and reaction time on the products indicated that the most important factor was the pH value of the reaction medium, which must be in between 2 to 6 to give zeolite crystals. The products have been characterized by XRD, SEM, DTA, IR, UV-Vis and N₂ adsorption techniques to be microporous zeolites, where Ti atoms are in complexation forms of TiO₄ and TiO₆. The Co titanate and Ga titanate zeolites had specific area of 263 and 204 m²/g, respectively.
- cobalt titanate,
- gallium titanate,
- molecular sieve,
- hydrothermal method
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