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Citation: ZHU Yun-Gui, LI Xue-Liang, HE Jian-Bo, LU Dao-Rong, QING Wei-Xing. The Effect of Aluminium on the Properties of Molybdenum Nitride Film Electrode[J]. Chinese Journal of Applied Chemistry, ;2001, 18(7): 540-543. shu

The Effect of Aluminium on the Properties of Molybdenum Nitride Film Electrode

1.
School of Chemical Engineering, Hefei University of Technology, Hefei 230009

Received Date: 28 August 2000
Available Online: 16 January 2001
Fund Project: 国家自然科学基金项目(29976009) (29976009)

The effect of aluminium on the property of molybdenum nitride film electrode has been studied by cyclic voltammetry, XRD and SEM.The results show that the quantity of Al₂(SO₄)3·6H₂O added strikingly influences the electrochemical behavior of the electrode prepared by dipping-calcination method.At optimum additive concentration in the dipping solution, the specific electric capacity of the electrode is 2.6 times that of the electrode prepared without additive in the dipping solution and the operating voltage value of the electrode increases by 0.13 V.The mechanism of aluminium affecting on the property of the film electrode is suggested that a lot of hole with size greater than 2 nm are formed in the film of the electrode, making the inner surface of the film wetted by the electrolyte solution and that there is an Al₁₁O₁₅N formed in the film of the electrode.
- molybdenum nitride electrode,
- aluminium sulfate,
- electrochemical behavior,
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