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Citation: ZENG Zhao-Hua, YANG Jian-Wen, QIN Hai-Ding, CHEN Yong-Lie. Study on Liquid Alkali Developing Type Solder Resists: Reaction Between Dibasic Acid Half-ester with Epoxy Compound[J]. Chinese Journal of Applied Chemistry, ;2002, 19(1): 18-21. shu

Study on Liquid Alkali Developing Type Solder Resists: Reaction Between Dibasic Acid Half-ester with Epoxy Compound

1.
Institute of Polymer Science, School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275

Corresponding author: ZENG Zhao-Hua,
Received Date: 22 May 2001
Available Online: 21 August 2001
Fund Project: 国家自然科学基金资助项目(59973027) (59973027)

Reaction of dibasic acid half-ester with epoxy compound has been investigated as function of factors affecting the reaction between carboxyl groups and epoxy using half-esters of a series of acid:maleic acid(MAM), succinic acid(SAM), phthalic acid(PAM), cis-1,2,3,6-tetrahydrophthalic acid(H4PAM) and cis-hexahydrophthalic acid(H6PAM), and phenyl glycidyl ether(PGE) as model compounds. It was found that higher reactivity would be achieved for the dibasic acid half-esters with smaller molecular size or stronger acidity. In the case of reaction between maleic acid monomethyl eater(MAM) and PGE, the catalytic activity of the catalysts decreased in the order of chromium acetylacetonate (CrAA) > tetramethyl ammonium bromide(TMAB) > 1-methylimidazole(MI) > N,N-dimethyl benzylamine(DMBA). The effects of solvent polarity and temperature on the reaction has also been examined.
- liquid alkali developing,
- solder resist,
- dibasic acid half-ester,
- epoxy
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