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Citation: PANG Xiu-Yan, SUN Han-Wen, LI Zhi-Yuan, ZHANG Hong-Juan. Synthesis of Ammonium Thiocyanate by Phase Transfer Catalysis[J]. Chinese Journal of Applied Chemistry, ;2002, 19(4): 407-408. shu

Synthesis of Ammonium Thiocyanate by Phase Transfer Catalysis

1.
College of Chemistry and Environmental Science, Hebei University, Baoding 071002

Corresponding author: PANG Xiu-Yan,
Received Date: 20 October 2001
Available Online: 3 February 2002

Ammonium thiocyanate was prepared in 2 steps from aqueous ammonia and carbon disulfied by phase transfer catalysis in yield of 72.7%, when catalysts consisted of OP-4 and OP-21 in mole ratio of 4:6. The effects of reaction temperature, time, mole ratio of OP-4 to OP-21 and conparison with other catalysts on the reaction were descurved.
- ammonium thiocyanate,
- preparerition,
- phase transfer catalysis
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