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Citation: SONG Jin-Yong, WANG Chao-Jie, ZHAO Jin, TANG Yan-Li, HUANG Xiao-Qin, SUN Xin-Qi. Synthesis of Solanesylamine Derivatives(Ⅰ)——Synthesis of N,N-Di(acyloxyethyl) solanesylamine[J]. Chinese Journal of Applied Chemistry, ;2002, 19(6): 600-602. shu

Synthesis of Solanesylamine Derivatives(Ⅰ)——Synthesis of N,N-Di(acyloxyethyl) solanesylamine

1.
College of Chemistry and Chemical Engineering, He'nan University, Kaifeng 475001

Corresponding author: WANG Chao-Jie,
Received Date: 8 August 2001
Available Online: 26 November 2001
Fund Project: 河南省科委攻关项目(0124090409) (0124090409)

Solanesyl bromide(Ⅱ) was reacted with diethanolamine to give solanesyl diethanolamine(Ⅲ) which was acylated with 3,4,5-trimethoxybenzoyl chloride, acetic anhydride, benzoyl chloride and cinnamyl chloride to give i>N,N-di[(3,4,5 trimethoxybenzoyloxy)ethyl]solanesylamine(Ⅳ), N,N-di[(acetyloxy)ethyl] solanesylamine(Ⅴ), i>N,N-di[(benzoyloxy)ethyl]solanesylamine(Ⅵ), i>N,N-di[(cinnyloxy)ethyl]solanesylamine(Ⅶ) respectively. The structures of compounds Ⅲ~Ⅶ were confirmed by IR, ¹H NMR, MS and elemental analysis.
- i>N,N-di(acyloxyethyl)solanesylamine,
- synthesis,
- solanesol
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