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Citation: YU Jiu-Gao, YANG Dong-Zhi. Preparation and Application of 3,5-Dinitrobenzoic Acid Ester of Starch[J]. Chinese Journal of Applied Chemistry, ;2002, 19(9): 858-861. shu

Preparation and Application of 3,5-Dinitrobenzoic Acid Ester of Starch

YU Jiu-Gao ^, ,
YANG Dong-Zhi

1.
Science School, Tianjin University, Tianjin 300072

Corresponding author: YU Jiu-Gao,
Received Date: 26 December 2001
Available Online: 26 April 2002

A novel starch derivative——3,5-dinitrobenzoic acid ester of starch(DNBZ-ST) with different degree of substitution(DS) was prepared by reaction of starch with 3,5-dinitrobenzoyl chloride. The structures of products were characterized by FTIR, elemental analysis, ¹³C NMR and TG. The best reaction conditions were given. The DNBZ-ST has a good adsorption property for creatinine. The highest adsorption capacity was 25.0 mg creatinine per gram of DNBZ-ST(DS=2.09) at 37℃, pH=7 and creatinine concentration in solution of 100 mg/L.
- starch,
- starch dinitrobenzoic acid ester,
- preparation,
- polymeric adsorbent
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