Citation:
ZHOU Lei, ZHAO Wen-Kuan, FANG You-Ling. Photocatalytic Activity of Anatase TiO2 Thin Films Prepared by Liquid Phase Deposition[J]. Chinese Journal of Applied Chemistry,
;2002, 19(10): 919-922.
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Anatase TiO2 thin films on glass substrate were obtained in an aqueous solution of (NH4)2TiF6 and H3BO3 supersaturated with nano-crystalline TiO2. When the concentration of TiF62- in the aqueous solution was 0.1 mol/L, and the TiF62-/H3BO3 molar ratio was 1:2~1:4 transparent anatase TiO2 thin films could be obtained by deposition at 35℃ followed by calcination. It is found that the film thickness increased with deposition time and achieved 260 nm at a deposition time of 9 h. The photocatalytic activity of the TiO2 thin films was evaluated through catalytic degradation of methylene blue. The TiO2 thin films prepared by calcination at 300℃ showed the strongest photocatalytic activity, which was 5 times the activity of the films prepared without calcination.
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