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Citation: CUI Bin, TIAN Chang-Sheng, SHI Qi-Zhen. Preparation of (1-x)Pb(Ni_1/3Nb_2/3)O₃-xPbTiO₃ Ceramics[J]. Chinese Journal of Applied Chemistry, ;2003, 20(2): 134-137. shu

Preparation of (1-x)Pb(Ni_1/3Nb_2/3)O₃-xPbTiO₃ Ceramics

1.
a Department of Chemistry, Northwest University, Shaanxi Provincial Key Laboratory of Physico-Inorganic Chemistry, Xi'an 710069;
2.
b College of Materials Science and Engineering, Northwest Polytechnical University, Xi'an 710072

Corresponding author: CUI Bin,
Received Date: 9 July 2002
Available Online: 12 November 2002
Fund Project: 陕西省自然科学基金(2001H06) (2001H06)西北大学科学基金(00NW41)资助项目 (00NW41)

The ferroelectric materials, (1-x)Pb(Ni_1/3Nb_2/3)O₃-xPbTiO₃[(1-x)PNN-xPT,x(PT)=0,0.15,0.25,0.36,0.45] were prepared from nickel nitrate instead of commonly used nickel oxide. The (1-x)PNN-xPT powders were prepared from the precursor, which was synthesized by adding an aqueous Ni(NO₃)₂ solution to the alcoholic slurry of PbO, Nb₂O₅ and TiO₂, followed by calcination at 850℃ for 3 h. Without the addition of excess NiO, the (1-x)PNN-xPT ceramics sintered at 1 100℃ for 2 h were dense and composed of only the perovskite phase. The ceramics exhibited better dielectric property than those obtained by Columbite precursor method.
- lead nickel niobate,
- perovskite phase,
- relaxor ferroelectric ceramics,
- synthesis
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Preparation of (1-x)Pb(Ni_1/3Nb_2/3)O₃-xPbTiO₃ Ceramics