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Citation: WANG Hai-Tang, SHI Qing-Liang, WANG Xiao-Wei, ZHANG Xin-Yi, ZHANG Wei-Yuan. Optimization of Technological Preparation Condition of Colloid Sb₂O₅ by Using Sodium Borate as Stabilizer[J]. Chinese Journal of Applied Chemistry, ;2003, 20(5): 496-498. shu

Optimization of Technological Preparation Condition of Colloid Sb₂O₅ by Using Sodium Borate as Stabilizer

1.
School of Chemical Engineering, He'nan University of Science & Technology, Luoyang 471003

Corresponding author: WANG Hai-Tang,
Received Date: 29 August 2002
Available Online: 31 December 2002
Fund Project: 河南省科技攻关项目(001090403) (001090403)

The technological process of preparation of colloid Sb₂O₅ by oxidation of Sb₂O₃ with hydrogen peroxide using borax as a stabilizer has been investigated.The optimum preparation conditions selected by orthogonal factorization method as follows m(H₂O):m(Sb₂O₃)=7.5:1,n(H₂O₂):n(Sb₂O₃)=3:1,m(Na₂B₄O₇·10H₂O):m(Sb₂O₃)=11:0,95℃,1.5 h.The conversion of Sb₂O₃>95%,light transmittance of colloid >85% and the average diameter of Sb₂O₅ particles was 50 nm.The colloid Sb₂O₅ prepared was storage stable without coagulation for more than one year.
- colloid antimony pentoxide,
- borax,
- stabilizer,
- preparation condition
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Optimization of Technological Preparation Condition of Colloid Sb₂O₅ by Using Sodium Borate as Stabilizer