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Citation: XIN Bing-Wei, SUN Chang-Jun, QU Li-Qiang, CAO Xiao-Ran. Synthesis of Glucosides XXⅠ Synthesis of 2-N-(β-D-Glucopyranos-1-yl)-6-(4-Halophenyl)-3-Pyridazinone[J]. Chinese Journal of Applied Chemistry, ;2003, 20(6): 590-593. shu

Synthesis of Glucosides XXⅠ Synthesis of 2-N-(β-D-Glucopyranos-1-yl)-6-(4-Halophenyl)-3-Pyridazinone

1.
a Department of Chemistry, Dezhou University, Dezhou 253023;
2.
b School of Chemistry and Chemical Engineering, Shandong Univeristy, Ji'nan

Corresponding author: XIN Bing-Wei,
Received Date: 18 September 2002
Available Online: 31 March 2003

Four pyridazinone glucosides 3 were synthesized by reaction of 2,3,4,6-tetra-O-acetyl-1-bromo-1-deoxy-α-D-glucopyranose 1 with 6-(4-halophenyl)-3(2H)-pyridazinone 2 under phase transfer catalysis conditions,followed by treatment with dry am monia at 0~-5℃ to yield title compounds 4.Their structures were characterized by IR,¹H NMR,¹³C NMR and elemental analysis.
- pyridazinone glucoside,
- synthesis,
- phase transfer catalysis
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