Citation:
LI Qing-Shan, ZHANG Jin-Chao, SONG Li, WANG Jun. Influence of Preparation Conditions on the Water-Dispersion of Sb/SnO2 Ultrafine Powder[J]. Chinese Journal of Applied Chemistry,
;2003, 20(11): 1076-1079.
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Sb/SnO2 ultrafine powder water-dispersion prepared by a ball-grinding method has been investigated as function of pH value, Sb concentration and calcination temperature by measurements of the Zeta potential and sedimentation rate of the dispersion. The results indicate that the Sb/SnO2 ultrafine powder dispersion is dependent on the preparation conditions through their effects on the surface state, chemical composition and crystal state of the final products. The zero Zeta potential point of the Sb/SnO2 ultrafine powder is about 1.8. The proper conditions for higher stable Sb/SnO2 ultrafine powder water-dispersion are: pH=10.0~11.5, n(Sb)/n(Sn) 0.04~0.19 and calcination temperature 800℃.
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