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Citation: WANG Ya-Qiong, TONG Hong-Yang, XU Wen-Lin. Effect of SnO₂+Sb₂O₃ Intermediate Layer on the Performance of Ti/SnO₂+Sb₂O₃/PbO₂ Anodes[J]. Chinese Journal of Applied Chemistry, ;2004, 21(5): 437-441. shu

Effect of SnO₂+Sb₂O₃ Intermediate Layer on the Performance of Ti/SnO₂+Sb₂O₃/PbO₂ Anodes

1.
College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002

Corresponding author: WANG Ya-Qiong,
Received Date: 27 February 2003
Available Online: 27 May 2003
Fund Project: 国家自然科学基金(20176047) (20176047)

The effects of calcination temperatures and Sb content in SnO₂+Sb₂O₃ intermediate layers prepared from polymeric precursor on the performance of the Ti/SnO₂+Sb₂O₃/PbO₂ anodes have been studied. The SnO₂+Sb₂O₃ intermediate layers were characterized by XRD,SEM and a probe method. The anode performance was assessed with the polarization curve, the cathodic voltammetric charge and the fast lifetime determinations in the 1.0 mol/L H₂SO₄ solution. It was found that calcination temperature and Sb content in SnO₂+Sb₂O₃ intermediate layer obviously affected the performance of the Ti/SnO₂+Sb₂O₃/PbO₂ anode. For anode containing intermediate layer calcinated at 500℃ and with n(Sn):n(Sb)=9:1 the anode life achived 30 h in 1.0 mol/L H₂SO₄ solutions and with good stability.
- Ti/PbO₂,
- SnO₂,
- Sb₃O₃ intermediate
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Effect of SnO₂+Sb₂O₃ Intermediate Layer on the Performance of Ti/SnO₂+Sb₂O₃/PbO₂ Anodes