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Citation: TANG Xu-Dong, CHEN Xiao-Ting, ZHANG Ming-Zhu, LU Hua-Gang, LI Zhuo-Peng. Synthesis and Spectral Properties of Di-Schiff Base Compounds Poly(ether ether ketone) with Bisphenol-A Moiety[J]. Chinese Journal of Applied Chemistry, ;2004, 21(10): 1051-1053. shu

Synthesis and Spectral Properties of Di-Schiff Base Compounds Poly(ether ether ketone) with Bisphenol-A Moiety

1.
School of Material Science & Chemical Engineering, Tianjin University of Science & Techology, Tianjin 300222

Corresponding author: TANG Xu-Dong,
Received Date: 29 September 2003
Available Online: 27 February 2004
Fund Project: 国家自然科学基金资助项目(50203008) (50203008)

A novel poly(ether ether ketone) derived from 2-(6-oxide-6H-dibenz〈1,2>oxa phospho rin-6-yl)-1,4-dihydroxyphenylene, 4,4'-diflourodiphenylketone and bisphenol-A was synthesized by solution polycondensation. The influences of reaction time, and concentration of reactants on the polymerization were investigated. A copolymer with inherent viscosity of 1.44 was obtained. As characterized by FT-IR, ¹H NMR and ³¹P NMR the product was a terpolymer, consisted of bisphenol A and difluorodiphenylketone. The DSC analysis show its T_g was 171℃. The copolymer was soluble in many polar solvents.
- poly(ether ether ketone),
- solution polycondensation,
- phosphorous monomer
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