Citation:
XU Xiu-Qin, CAI Duo-Chang, ZOU Ru-Yi, HE Xiao-Ying. Quantitative Analysis of Vitamin B6 by Cyclic Voltammetry[J]. Chinese Journal of Applied Chemistry,
;2004, 21(10): 1016-1019.
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The carboxylated MWNT was dispersed in acetone and a drop of the suspension on GCE was dried to yield a multi-wall carbon nanotube modified glassy carbon electrode(MWNT/GCME). Vitamin B6 could be directly determined using the MWNT/GCME as working electorde by cyclic voltammetry in a buffer solution of NH4Cl-NH3·H2O(pH=8.0). The results showed that the peak current was proportional to the concentration of VB6 over the concentration range of 1.0×10-6 to 1.0×10-3 mol/L at the scan rate of 100 mV/s, and the detection limit was 1.0×10-6 mol/L with a correlation coeffecient of 0.998. Using this modified electrode, the VB6 content in a VB6 tablet was determined satisfactorily.
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