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Citation: ZHANG Wei, ZHAO De-Feng. Synthesis and Coloration Properties of a Universal Dye Containing Two Naphthalene Rings[J]. Chinese Journal of Applied Chemistry, ;2005, 22(2): 123-127. shu

Synthesis and Coloration Properties of a Universal Dye Containing Two Naphthalene Rings

ZHANG Wei ,
ZHAO De-Feng ^,

1.
State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian 116012

Corresponding author: ZHAO De-Feng,
Received Date: 6 April 2004
Available Online: 16 July 2004
Fund Project: 国家自然科学基金资助项目(20172012) (20172012)

A new universal dye containing two naphthalene rings was prepared by condensation of 7-aceta-mide-4-hydroxy-2-naphthalene sulfonyl chloride with N,N-dimethylethylenediamine, followed by the coupling reaction with ammonium of m-amino-benzene-β-hydroxyethylene sulfonate. The chemical structures of the new dye and the intermediate were confirmed by Mass Spectrometry, ¹H NMR and ¹³C NMR analyses. By adjusting the pH value of the dyebath and adding textile auxiliaries, the synthesized universal dye was applied to dye cotton, wool, silk, nylon, acrylic and PET fabrics without conducting other chemical reactions outside the dyebath. The exhaustion rates of dye on the fabrics aforementioned were 6.2%, 59.8%, 44.7%, 33.5%, 11.1% and 9.2%, respectively, which reveals that the dye has good affinity for wool, silk and nylon fabrics. The washfastness grades of dyed wool, silk and nylon fabrics were all higher than 3, while their lightfastness properties were not satisfactory.
- universal dye,
- naphthalene ring,
- synthesis,
- coloration property
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