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Citation: WANG Wei, WU Qun-Rong, YANG Zhi-Lan, SHEN Chang-Hong, ZHANG Ai-Qing, WEI Hai-Yang. Synthesis of 3,3'-Diaminochalcone[J]. Chinese Journal of Applied Chemistry, ;2006, 23(4): 447-449. shu

Synthesis of 3,3'-Diaminochalcone

1.
College of Chemistry and Material Science, South-Central University for Nationalities, Wuhan 430074

Corresponding author: ZHANG Ai-Qing,
Received Date: 12 June 2005
Available Online: 10 August 2005
Fund Project: 国家自然科学基金项目(50373052) (50373052)湖北省自然科学基金重点项目(2001ABA009) (2001ABA009)

3,3'-Dinitrochalcone was synthesized by the Claisen-Schmidt condensation of nitrobenzaldehyde and nitroacetophenone,which was reduced to 3,3'-diaminochalcone by 85% hydrazine hydration with FeCl₃·6H₂O/C.The product was characterized by elemental analysis,melting point,IR,and ¹H NMR measurements.The factors influencing the product yield were also discussed.Co MPared with previous methods in the literature,the present procedure has the advantages of milder conditions,lower cost,easier work-up,high product yield(78.6%) and is environmental friendly.
- photosensitive diamine,
- chalcone,
- polyimide,
- synthesis
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