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Citation: ZHANG Feng, SUN Ji-Kui, LI Ya-Zhuo, GAO Da-Wei, ZHANG Yu-Min, ZHAO Tian-Qi, CHEN Xiao-Dong. Synthesis of Monoester Compounds of Furoin[J]. Chinese Journal of Applied Chemistry, ;2007, 24(12): 1461-1463. shu

Synthesis of Monoester Compounds of Furoin

1.
a College of Chemistry, Jilin University, Changchun 130012;
2.
b Analytical Center of Jilin University, Changchun

Corresponding author: GAO Da-Wei,
Received Date: 7 January 2007
Available Online: 5 March 2007
Fund Project: 吉林省科技厅资助项目(1999010540) (1999010540)

Furoin was synthesized from furol with VB₁ as the catalyst,which was then reacted with acetyl chloride,lauroyl chloride,benzoyl chloride,α-furoyl chloride and 3-α-furyl acryloyl chloride,respectively;corresponding monoester compounds of furoin were synthesized in THF in the presence of sodium hydroxide under reflux.The yields of compounds 1,2,3,4,and 5 based on furoin were 99.3%,96.5%,98.0%,99.4% and 98.7%,respectively.By characterization with elementary analysis,Mass spectrum and ¹H NMR,the structures of the target products were characterized by elemental analysis,MS and ¹H NMR.
- furoin,
- acetyl chloride,
- lauroyl chloride,
- benzoyl chloride,
- α-furoyl chloride,
- α-furyl acryloyl chloride,
- esterification,
- synthesis
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