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Citation: HUANG Bao-Mei, YAO Cheng-Wei, WANG Xiu-Feng, WANG Zhi-Guo, MO Jin-Yuan. Determination of Antipyrinum and Amidopyrine by Capillary Electrophoresis with Amperometric Detection[J]. Chinese Journal of Applied Chemistry, ;2008, 25(2): 241-244. shu

Determination of Antipyrinum and Amidopyrine by Capillary Electrophoresis with Amperometric Detection

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a Chemical Department of Mian Yang Normal University, MianYang 621000;
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b The 4th Institute of CARDC, MianYang;
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c School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou

Corresponding author: HUANG Bao-Mei,
Received Date: 15 March 2007
Available Online: 24 July 2007

On the self-constructed electrochemical detection system,antipyrinum and amidopyrine in injection antondint were separated and determined by capillary electrophoresis with amperometric detection(CE-AD).Under the optimized conditions:a running buffer composed of 30 mmol/L Na₂B₄O₇ buffer pH 9.0,separation voltage 20 kV,injection time 8 seconds and detection voltage 0.8 V,a linear relationaships between peak areas(Y) and mass concentrations(c) of the two analytes were established,with a determination limit of 0.1 mg/L for antipyrinum and that of 0.05 mg/L for amidopyrine,respectively.
- capillary electrophoresis,
- injection antondint,
- antipyrinum,
- amidopyrine,
- amperometric detection
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