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Citation: SONG Wei-Ming, HU Qi-Lin, FANG Jun-Zhuo, NI Gang, LUO Min. PEG-assisted Synthesis of Tin-doped Indium Oxide Nanopowders by Sol-gel Method[J]. Chinese Journal of Applied Chemistry, ;2008, 25(4): 464-467. shu

PEG-assisted Synthesis of Tin-doped Indium Oxide Nanopowders by Sol-gel Method

SONG Wei-Ming ^a,, ,
HU Qi-Lin ^a ,
FANG Jun-Zhuo ^b ,
NI Gang ^a ,
LUO Min ^a

1.
a School of chemistry and Chemical Engineering, Ningxia University, Yinchuan 750021;
2.
b Key Laboratory of Energy Sources and Chemical Engineering, Ningxia University, Yinchuan

Corresponding author: SONG Wei-Ming,
Received Date: 28 April 2007
Available Online: 29 August 2007
Fund Project: 宁夏回族自治区教育厅宁夏高等学校科学技术研究(2005) (2005)宁夏自然科学基金(NZ0718)资助项目 (NZ0718)

The water-based sol-gel method was applied to synthesize indium tin oxide (ITO) nanoparticles with m(In):m(Sn)=90:10 with polyethylene glycol (PEG) 20000 as a dispersant.The pyrolytic behavior of the dried gel and formation process of ITO were investigated by TG-DTA and XRD.The particle morphology,specific surface area and crystal size of the as-synthesized ITO powders were investigated by TEM and BET.The results indicate that monodispersed ITO nanopowers were synthesized after dried gel was calcined at 500℃.The as-synthesized sample was cubic phase In₂O₃ structure with a special surface area of 50 m²/g and a particle diameter of (15±5) nm,which is in good agreement with the observation of TEM,XRD and BET.The proposed technique has a significant potential for the commercial production of ITO nanopowders.
- Indium tin oxide,
- PEG-assisted sol-gel method,
- Nanoparticle
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